N'-(6-(2-(2-hydroxyethoxy)ethoxy)hexyl)-N,N-dimethylacetimidamide

Base Information

• Chemical Name: N'-(6-(2-(2-hydroxyethoxy)ethoxy)hexyl)-N,N-dimethylacetimidamide
• CAS No.: 1268136-23-7
• Molecular Formula: C₁₄H₃₀N₂O₃
• Molecular Weight: 274.404

Synonyms:N'-(6-(2-(2-hydroxyethoxy)ethoxy)hexyl)-N,N-dimethylacetimidamide

Chemical Property of N'-(6-(2-(2-hydroxyethoxy)ethoxy)hexyl)-N,N-dimethylacetimidamide

Chemical Property:

Purity/Quality:

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Technology Process of N'-(6-(2-(2-hydroxyethoxy)ethoxy)hexyl)-N,N-dimethylacetimidamide

There total 1 articles about N'-(6-(2-(2-hydroxyethoxy)ethoxy)hexyl)-N,N-dimethylacetimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-phthalimido-1-hexanol (63945-11-9) → N'-(6-(2-(2-hydroxyethoxy)ethoxy)hexyl)-N,N-dimethylacetimidamide (1268136-23-7)

Guidance literature:

Multi-step reaction with 5 steps

1.1: dmap / dichloromethane / 20 °C

1.2: 18 h / 20 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / Inert atmosphere

2.2: 18 h / 65 °C / Inert atmosphere

3.1: palladium 10% on activated carbon; hydrogen / ethanol / 6 h / 20 °C

4.1: hydrazine hydrate / ethanol / 3 h / 76 °C

4.2: 3 h / 76 °C

5.1: 1-aminodecane; dimethyl amine / tetrahydrofuran / 18.25 h / 20 °C / Darkness

With dmap; hydrazine hydrate; 1-aminodecane; palladium 10% on activated carbon; hydrogen; sodium hydride; dimethyl amine; In tetrahydrofuran; ethanol; dichloromethane; mineral oil; 2.1: Williamson synthesis / 2.2: Williamson synthesis;

DOI:10.1021/jo102358d

upstream raw materials:

6-phthalimido-1-hexanol

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