Gxkqoeygynaibb-uhfffaoysa-

Base Information

Chemical Name:Gxkqoeygynaibb-uhfffaoysa-
CAS No.:331714-63-7
Molecular Formula:C₁₁H₈N₂O₂
Molecular Weight:200.197
Hs Code.:
DSSTox Substance ID:DTXSID701243547

Synonyms:GXKQOEYGYNAIBB-UHFFFAOYSA-;DTXSID701243547;2-(1,3-Dioxolan-2-yl)-1,3-benzenedicarbonitrile;331714-63-7;InChI=1/C11H8N2O2/c12-6-8-2-1-3-9(7-13)10(8)11-14-4-5-15-11/h1-3,11H,4-5H2

Suppliers and Price of Gxkqoeygynaibb-uhfffaoysa-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Gxkqoeygynaibb-uhfffaoysa-

Chemical Property:

XLogP3:0.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:200.058577502
Heavy Atom Count:15
Complexity:294

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1COC(O1)C2=C(C=CC=C2C#N)C#N

Technology Process of Gxkqoeygynaibb-uhfffaoysa-

There total 5 articles about Gxkqoeygynaibb-uhfffaoysa- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 544-92-3
copper(I) cyanide

: 331714-62-6
2-(2,6-dibromophenyl)-1,3-dioxolane

: 331714-63-7
2-(2,6-dicyanophenyl)-1,3-dioxolane

Guidance literature:: In N,N-dimethyl-formamide; at 150 ℃;
DOI:10.1002/1099-0690(200101)2001:2<293::AID-EJOC293<3.0.CO;2-N

Reference yield:

: 67713-23-9
2,6-dibromobenzaldehyde

: 331714-63-7
2-(2,6-dicyanophenyl)-1,3-dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / p-toluenesulfonic acid / toluene / Heating

2: 59 percent / dimethylformamide / 150 °C

With toluene-4-sulfonic acid; In N,N-dimethyl-formamide; toluene; 2: Rosenmund-von Braun reaction;
DOI:10.1002/1099-0690(200101)2001:2<293::AID-EJOC293<3.0.CO;2-N

Reference yield:

: 55289-36-6
3-bromo-2-methylaniline

: 331714-63-7
2-(2,6-dicyanophenyl)-1,3-dioxolane

Guidance literature:: Multi-step reaction with 4 steps

1.1: NaNO₂

1.2: CuBr

2.1: CrO₃; H₂SO₄ / acetic acid; acetic anhydride

2.2: H₂SO₄ / ethanol / 80 °C

3.1: 74 percent / p-toluenesulfonic acid / toluene / Heating

4.1: 59 percent / dimethylformamide / 150 °C

With chromium(VI) oxide; sulfuric acid; toluene-4-sulfonic acid; sodium nitrite; In acetic anhydride; acetic acid; N,N-dimethyl-formamide; toluene; 4.1: Rosenmund-von Braun reaction;
DOI:10.1002/1099-0690(200101)2001:2<293::AID-EJOC293<3.0.CO;2-N