D-1,2-O-isopropylidene-5-O-benzoyl-6-O-benzyl-myo-inositol 3,4-bis(dibenzylphosphate)

Base Information

Chemical Name:D-1,2-O-isopropylidene-5-O-benzoyl-6-O-benzyl-myo-inositol 3,4-bis(dibenzylphosphate)
CAS No.:956031-51-9
Molecular Formula:C₅₁H₅₂O₁₃P₂
Molecular Weight:934.914
Hs Code.:

Synonyms:D-1,2-O-isopropylidene-5-O-benzoyl-6-O-benzyl-myo-inositol 3,4-bis(dibenzylphosphate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of D-1,2-O-isopropylidene-5-O-benzoyl-6-O-benzyl-myo-inositol 3,4-bis(dibenzylphosphate)

Chemical Property:

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Technology Process of D-1,2-O-isopropylidene-5-O-benzoyl-6-O-benzyl-myo-inositol 3,4-bis(dibenzylphosphate)

There total 12 articles about D-1,2-O-isopropylidene-5-O-benzoyl-6-O-benzyl-myo-inositol 3,4-bis(dibenzylphosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₆H₁₀O₄(C₃H₄)(C₇H₆)H₂COC₆H₄(PO₃C₁₄H₁₃)2

: 956031-51-9
D-1,2-O-isopropylidene-5-O-benzoyl-6-O-benzyl-myo-inositol 3,4-bis(dibenzylphosphate)

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1080/07328300701540225

Reference yield:

: 100-39-0
benzyl bromide

: 956031-51-9
D-1,2-O-isopropylidene-5-O-benzoyl-6-O-benzyl-myo-inositol 3,4-bis(dibenzylphosphate)

Guidance literature:: Multi-step reaction with 9 steps

1: 91.3 percent / NaH; TBAI / tetrahydrofuran / 0 - 20 °C

2: 89.2 percent / NMO / OsO₄ / acetone; H₂O / 12 h / 20 °C

3: TSA / CH₂Cl₂ / 1 h / 20 °C

4: 2.0 g / H₂; NaHCO₃ / Pd/C / tetrahydrofuran / 72 h / 20 °C / 760.05 Torr

5: 97.7 percent / DMAP; pyridine / 6 h / 20 °C

6: 68.5 percent / TSA / methanol; CH₂Cl₂ / 15 h / 0 °C

7: 23.8 percent / pyridine / H₂O / 10 h / 90 °C

8: 1H-tetrazole / dimethylformamide; CH₂Cl₂ / 7 h / 20 °C

9: m-CPBA / dimethylformamide; CH₂Cl₂ / 0 - 20 °C

With pyridine; 1H-tetrazole; dmap; N-methyl-2-indolinone; hydrogen; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; osmium(VIII) oxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1080/07328300701540225

Reference yield:

: 176200-07-0
(3aS,4S,4aR,7aR,8S,8aR)-4,8-Bis-benzyloxy-2,2,6,6-tetramethyl-hexahydro-benzo[1,2-d;4,5-d']bis[1,3]dioxole

: 956031-51-9
D-1,2-O-isopropylidene-5-O-benzoyl-6-O-benzyl-myo-inositol 3,4-bis(dibenzylphosphate)

Guidance literature:: Multi-step reaction with 6 steps

1: 2.0 g / H₂; NaHCO₃ / Pd/C / tetrahydrofuran / 72 h / 20 °C / 760.05 Torr

2: 97.7 percent / DMAP; pyridine / 6 h / 20 °C

3: 68.5 percent / TSA / methanol; CH₂Cl₂ / 15 h / 0 °C

4: 23.8 percent / pyridine / H₂O / 10 h / 90 °C

5: 1H-tetrazole / dimethylformamide; CH₂Cl₂ / 7 h / 20 °C

6: m-CPBA / dimethylformamide; CH₂Cl₂ / 0 - 20 °C

With pyridine; 1H-tetrazole; dmap; hydrogen; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1080/07328300701540225