4-O-[2,3,4,6-tetrakis-O-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-1-O-(tert-butyldimethylsilyl)-2,3,6-tris-O-(4-methoxyphenylmethyl)-D-glucitol

Base Information

• Chemical Name: 4-O-[2,3,4,6-tetrakis-O-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-1-O-(tert-butyldimethylsilyl)-2,3,6-tris-O-(4-methoxyphenylmethyl)-D-glucitol
• CAS No.: 1315206-30-4
• Molecular Formula: C₇₄H₉₄O₁₈Si
• Molecular Weight: 1299.64

Synonyms:4-O-[2,3,4,6-tetrakis-O-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-1-O-(tert-butyldimethylsilyl)-2,3,6-tris-O-(4-methoxyphenylmethyl)-D-glucitol

Chemical Property of 4-O-[2,3,4,6-tetrakis-O-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-1-O-(tert-butyldimethylsilyl)-2,3,6-tris-O-(4-methoxyphenylmethyl)-D-glucitol

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Technology Process of 4-O-[2,3,4,6-tetrakis-O-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-1-O-(tert-butyldimethylsilyl)-2,3,6-tris-O-(4-methoxyphenylmethyl)-D-glucitol

There total 1 articles about 4-O-[2,3,4,6-tetrakis-O-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-1-O-(tert-butyldimethylsilyl)-2,3,6-tris-O-(4-methoxyphenylmethyl)-D-glucitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

4-O-[2,3,4,6-tetrakis-O-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-2,3,6-tris-O-(4-methoxyphenylmethyl)-D-glucitol (1315205-68-5) + tert-butyldimethylsilyl chloride (18162-48-6) → 4-O-[2,3,4,6-tetrakis-O-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-1-O-(tert-butyldimethylsilyl)-2,3,6-tris-O-(4-methoxyphenylmethyl)-D-glucitol (1315206-30-4)

Guidance literature:

With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1016/j.bmc.2011.04.048

Reference yield: 94.0%

4-O-[2,3,4,6-tetrakis-O-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-1-O-(tert-butyldimethylsilyl)-2,3,6-tris-O-(4-methoxyphenylmethyl)-D-glucitol (1315206-30-4) → (3S,4R,5S)-6-(tert-butyldimethylsilyloxy)-1,4,5-tris-O-(4-methoxyphenylmethyl)-2-oxohexan-3-yl 2,3,5-tris-O-(4-methoxyphenylmethyl)-β-D-glucopyranoside (1315206-32-6)

Guidance literature:

With acetic anhydride; dimethyl sulfoxide; at 20 ℃; for 12h; Inert atmosphere;

DOI:10.1016/j.bmc.2011.04.048

upstream raw materials:

4-O-[2,3,4,6-tetrakis-O-(4-methoxyphenylmethyl)-β-D-glucopyranosyl]-2,3,6-tris-O-(4-methoxyphenylmethyl)-D-glucitol

tert-butyldimethylsilyl chloride

Downstream raw materials:

(3S,4R,5S)-6-(tert-butyldimethylsilyloxy)-1,4,5-tris-O-(4-methoxyphenylmethyl)-2-oxohexan-3-yl 2,3,5-tris-O-(4-methoxyphenylmethyl)-β-D-glucopyranoside

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