[Mn(N,N-bis(2-pyridylmethyl)amine-N-ethyl-2-pyridine-2-carboxamide^(1-))(OPh)](ClO₄)

Base Information

• Chemical Name: [Mn(N,N-bis(2-pyridylmethyl)amine-N-ethyl-2-pyridine-2-carboxamide^(1-))(OPh)](ClO₄)
• CAS No.: 870248-75-2
• Molecular Formula: C₂₆H₂₅MnN₅O₂*ClO₄
• Molecular Weight: 593.905

Synonyms:[Mn(N,N-bis(2-pyridylmethyl)amine-N-ethyl-2-pyridine-2-carboxamide^(1-))(OPh)](ClO₄)

Chemical Property of [Mn(N,N-bis(2-pyridylmethyl)amine-N-ethyl-2-pyridine-2-carboxamide^(1-))(OPh)](ClO₄)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [Mn(N,N-bis(2-pyridylmethyl)amine-N-ethyl-2-pyridine-2-carboxamide^(1-))(OPh)](ClO₄)

There total 2 articles about [Mn(N,N-bis(2-pyridylmethyl)amine-N-ethyl-2-pyridine-2-carboxamide^(1-))(OPh)](ClO₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

[(Mn(N,N-bis(2-pyridylmethyl)amine-N-ethyl-2-pyridine-2-carboxamide(1-)))2(μ-O)](ClO4)2*2.7CH2Cl2*0.5CH3CN + phenol (108-95-2,27073-41-2) → [Mn(N,N-bis(2-pyridylmethyl)amine-N-ethyl-2-pyridine-2-carboxamide(1-))(OPh)](ClO4) (870248-75-2)

Guidance literature:

In acetonitrile; soln. PhOH in MeCN was addded to solnn. Mn complex in MeCN and stirred for 30 min; solvent was removed, residue was ecrystd. from CH2Cl2-toluene; elem. anal.;

DOI:10.1021/ic0503535

Reference yield: 65.0%

N,N-bis(2-pyridylmethyl)amine-N'-ethyl-2-pyridine-2-carboxamide (349649-58-7) + [Mn(DMF)6](ClO4)3 + sodium phenoxide (139-02-6) → [Mn(N,N-bis(2-pyridylmethyl)amine-N-ethyl-2-pyridine-2-carboxamide(1-))(OPh)](ClO4) (870248-75-2)

Guidance literature:

With sodium hydride; In acetonitrile; under N2 atm. to soln. ligand in MeCN NaH was added and stirred for 1 h,(Mn(DMF)6)(ClO4)3 was added and stirred for 2 h, soln. PhONa in MeCN wa s added; solvent was removed, residue was dissolved in CH2Cl2 and evapd. slowly;

DOI:10.1021/ic0503535

upstream raw materials:

N,N-bis(2-pyridylmethyl)amine-N'-ethyl-2-pyridine-2-carboxamide

sodium phenoxide

phenol

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 870248-75-2 [Mn(N,N-bis(2-pyridylmethyl)amine-N-ethyl-2-pyridine-2-carboxamide^(1-))(OPh)](ClO₄)

Send

Send

Metric Ton KG G Pound L ML

Send

Send