2,2-di-tert-butyl-2-chloro-4-(p-fluorophenyl)-4-(trifluoromethyl)-1,2λ⁵-oxaphosphetane

Base Information

• Chemical Name: 2,2-di-tert-butyl-2-chloro-4-(p-fluorophenyl)-4-(trifluoromethyl)-1,2λ⁵-oxaphosphetane
• CAS No.: 97939-27-0
• Molecular Formula: C₁₇H₂₄ClF₄OP
• Molecular Weight: 386.797

Synonyms:2,2-di-tert-butyl-2-chloro-4-(p-fluorophenyl)-4-(trifluoromethyl)-1,2λ⁵-oxaphosphetane

Chemical Property of 2,2-di-tert-butyl-2-chloro-4-(p-fluorophenyl)-4-(trifluoromethyl)-1,2λ⁵-oxaphosphetane

Chemical Property:

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Technology Process of 2,2-di-tert-butyl-2-chloro-4-(p-fluorophenyl)-4-(trifluoromethyl)-1,2λ⁵-oxaphosphetane

There total 1 articles about 2,2-di-tert-butyl-2-chloro-4-(p-fluorophenyl)-4-(trifluoromethyl)-1,2λ⁵-oxaphosphetane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2,2,2-trifluoro-1-(4-fluorophenyl)ethanone (655-32-3) + chlore-methylene-di(tert-butyle)phosphorane (76711-20-1) → 2,2-di-tert-butyl-2-chloro-4-(p-fluorophenyl)-4-(trifluoromethyl)-1,2λ5-oxaphosphetane (97939-27-0)

Guidance literature:

In diethyl ether; for 0.25h; Ambient temperature;

Reference yield: 85.0%

2,2-di-tert-butyl-2-chloro-4-(p-fluorophenyl)-4-(trifluoromethyl)-1,2λ5-oxaphosphetane (97939-27-0) → di-tert-butyl<3,3,3-trifluoro-2-(p-fluorophenyl)-2-hydroxypropyl>phosphine oxide

Guidance literature:

With water; In diethyl ether; moisture from air;

Reference yield: 70.0%

2,2-di-tert-butyl-2-chloro-4-(p-fluorophenyl)-4-(trifluoromethyl)-1,2λ5-oxaphosphetane (97939-27-0) → di-tert-butyl-<2-chloro-3,3,3-trifluoro-2-(p-fluorophenyl)propyl>phosphine oxide

Guidance literature:

With aluminium trichloride; In chloroform; for 0.0833333h;

upstream raw materials:

2,2,2-trifluoro-1-(4-fluorophenyl)ethanone

chlore-methylene-di(tert-butyle)phosphorane

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