tert-butyl 5-methyl-3-[1(R)-phenylethyl]-3-azabicyclo[3.1.0]hexan-1-ylcarbamate

Base Information

Chemical Name:tert-butyl 5-methyl-3-[1(R)-phenylethyl]-3-azabicyclo[3.1.0]hexan-1-ylcarbamate
CAS No.:1257389-90-4
Molecular Formula:C₁₉H₂₈N₂O₂
Molecular Weight:316.444
Hs Code.:

Synonyms:tert-butyl 5-methyl-3-[1(R)-phenylethyl]-3-azabicyclo[3.1.0]hexan-1-ylcarbamate

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Chemical Property of tert-butyl 5-methyl-3-[1(R)-phenylethyl]-3-azabicyclo[3.1.0]hexan-1-ylcarbamate

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Technology Process of tert-butyl 5-methyl-3-[1(R)-phenylethyl]-3-azabicyclo[3.1.0]hexan-1-ylcarbamate

There total 1 articles about tert-butyl 5-methyl-3-[1(R)-phenylethyl]-3-azabicyclo[3.1.0]hexan-1-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1257389-89-1
5-methyl-3-[1(R)-phenylethyl]-3-azabicyclo[3.1.0]hexan-1-amine

: 1257389-90-4
tert-butyl 5-methyl-3-[1(R)-phenylethyl]-3-azabicyclo[3.1.0]hexan-1-ylcarbamate

Guidance literature:: With sodium hydroxide; In water; at 20 ℃; for 21h;

Reference yield: 56.0%

: 1257389-90-4
tert-butyl 5-methyl-3-[1(R)-phenylethyl]-3-azabicyclo[3.1.0]hexan-1-ylcarbamate

: 74-88-4
methyl iodide

: 1257389-91-5
tert-butyl 5-methyl-3-[1(R)-phenylethyl]-3-azabicyclo[3.1.0]hexan-1-yl-N-methylcarbamate

Guidance literature:: tert-butyl 5-methyl-3-[1(R)-phenylethyl]-3-azabicyclo[3.1.0]hexan-1-ylcarbamate; With sodium hydride; In tetrahydrofuran; for 0.5h;

methyl iodide; In tetrahydrofuran; at 20 ℃; for 18h;