6-N-(benzyloxycarbonyl)-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyadenosine

Base Information

Chemical Name:6-N-(benzyloxycarbonyl)-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyadenosine
CAS No.:82995-78-6
Molecular Formula:C₃₀H₄₇N₅O₅Si₂
Molecular Weight:613.905
Hs Code.:

Synonyms:6-N-(benzyloxycarbonyl)-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyadenosine

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Chemical Property of 6-N-(benzyloxycarbonyl)-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyadenosine

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Technology Process of 6-N-(benzyloxycarbonyl)-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyadenosine

There total 8 articles about 6-N-(benzyloxycarbonyl)-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyadenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 51549-32-7
3',5'-bis-O-[(tert-butyl)dimethylsilyl]-2'-deoxyadenosine

: 82892-54-4
1-(benzyloxycarbonyl)-3-ethylimidazolium tetrafluoroborate

: 82995-78-6
6-N-(benzyloxycarbonyl)-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyadenosine

Guidance literature:: With sodium hydrogencarbonate; In chloroform; Ambient temperature;
DOI:10.1021/jo00144a014

Reference yield: 50.0%

: 83005-46-3
3',5'-bis-O-(tert-butyldimethylsiliyl)-2'-deoxy-6-N-<(methylthio)carbonyl>adenosine

: 100-51-6,185532-71-2
benzyl alcohol

: 82995-78-6
6-N-(benzyloxycarbonyl)-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyadenosine

Guidance literature:: With pyridine; silver nitrate; Ambient temperature;
DOI:10.1021/jo00144a014

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 82995-78-6
6-N-(benzyloxycarbonyl)-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyadenosine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) imidazole, 2.) 80percent aq. acetic acid / 1.) pyridine, room temperature, 2 d, 2.) room temperature, 30 min

2: CH₂Cl₂ / 15 h / Ambient temperature

With 1H-imidazole; acetic acid; In dichloromethane;
DOI:10.1021/ja00385a026