2-[3-fluoro-4-(phosphonooxy)phenyl]-7~vinyl-1,3-benzoxazol-5-yl dihydrogen phosphate

Base Information

Chemical Name:2-[3-fluoro-4-(phosphonooxy)phenyl]-7~vinyl-1,3-benzoxazol-5-yl dihydrogen phosphate
CAS No.:1178586-96-3
Molecular Formula:C₁₅H₁₂FNO₉P₂
Molecular Weight:431.208
Hs Code.:

Synonyms:2-[3-fluoro-4-(phosphonooxy)phenyl]-7~vinyl-1,3-benzoxazol-5-yl dihydrogen phosphate

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Chemical Property of 2-[3-fluoro-4-(phosphonooxy)phenyl]-7~vinyl-1,3-benzoxazol-5-yl dihydrogen phosphate

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Technology Process of 2-[3-fluoro-4-(phosphonooxy)phenyl]-7~vinyl-1,3-benzoxazol-5-yl dihydrogen phosphate

There total 2 articles about 2-[3-fluoro-4-(phosphonooxy)phenyl]-7~vinyl-1,3-benzoxazol-5-yl dihydrogen phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1178586-95-2
2-{4-[(diethoxyphosphoryl)oxy]-3-fluorophenyl}-7-vinyl-1,3-benzoxazol-5-yl diethyl phosphate

: 1178586-96-3
2-[3-fluoro-4-(phosphonooxy)phenyl]-7~vinyl-1,3-benzoxazol-5-yl dihydrogen phosphate

Guidance literature:: 2-{4-[(diethoxyphosphoryl)oxy]-3-fluorophenyl}-7-vinyl-1,3-benzoxazol-5-yl diethyl phosphate; With trimethylsilyl bromide; at 20 ℃; for 72h;

With water; In diethyl ether; for 0.5h;

Reference yield:

: 524684-52-4
prinaberel

: 1178586-96-3
2-[3-fluoro-4-(phosphonooxy)phenyl]-7~vinyl-1,3-benzoxazol-5-yl dihydrogen phosphate

Guidance literature:: Multi-step reaction with 2 steps

1.1: dmap; N-ethyl-N,N-diisopropylamine / tetrahydrofuran; tetrachloromethane; acetonitrile / 8 h / 20 °C

2.1: trimethylsilyl bromide / 72 h / 20 °C

2.2: 0.5 h

With dmap; trimethylsilyl bromide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; tetrachloromethane; acetonitrile;