2-chloromethyl-3-carboethoxy-5-carbomethoxy-4-(m-nitrophenyl)-6-methylpyridine

Base Information

Chemical Name:2-chloromethyl-3-carboethoxy-5-carbomethoxy-4-(m-nitrophenyl)-6-methylpyridine
CAS No.:118587-21-6
Molecular Formula:C₁₈H₁₇ClN₂O₆
Molecular Weight:392.796
Hs Code.:

Synonyms:2-chloromethyl-3-carboethoxy-5-carbomethoxy-4-(m-nitrophenyl)-6-methylpyridine

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Chemical Property of 2-chloromethyl-3-carboethoxy-5-carbomethoxy-4-(m-nitrophenyl)-6-methylpyridine

Chemical Property:

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Technology Process of 2-chloromethyl-3-carboethoxy-5-carbomethoxy-4-(m-nitrophenyl)-6-methylpyridine

There total 5 articles about 2-chloromethyl-3-carboethoxy-5-carbomethoxy-4-(m-nitrophenyl)-6-methylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121236-58-6
(3S,4R)-2-[1-Chloro-meth-(Z)-ylidene]-6-methyl-4-(3-nitro-phenyl)-1,2,3,4-tetrahydro-pyridine-3,5-dicarboxylic acid 3-ethyl ester 5-methyl ester

: 118587-21-6
2-chloromethyl-3-carboethoxy-5-carbomethoxy-4-(m-nitrophenyl)-6-methylpyridine

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In pyridine; Ambient temperature;
DOI:10.1016/S0040-4039(00)82340-0

Reference yield:

: 638-07-3
ethyl (2-chloroaceto)acetate

: 118587-21-6
2-chloromethyl-3-carboethoxy-5-carbomethoxy-4-(m-nitrophenyl)-6-methylpyridine

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / piperidine acetate / benzene / Heating; azeotr. rem. of water

2: ethanol / 0.33 h / Heating

3: CHCl₃ / 0.08 h / Ambient temperature; acidic EtOH

4: DDQ / pyridine / Ambient temperature

With piperdinium acetate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In pyridine; ethanol; chloroform; benzene;
DOI:10.1016/S0040-4039(00)82340-0

Reference yield:

: 99-61-6
3-nitro-benzaldehyde

: 118587-21-6
2-chloromethyl-3-carboethoxy-5-carbomethoxy-4-(m-nitrophenyl)-6-methylpyridine

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / piperidine acetate / benzene / Heating; azeotr. rem. of water

2: ethanol / 0.33 h / Heating

3: CHCl₃ / 0.08 h / Ambient temperature; acidic EtOH

4: DDQ / pyridine / Ambient temperature

With piperdinium acetate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In pyridine; ethanol; chloroform; benzene;
DOI:10.1016/S0040-4039(00)82340-0