3endo-t-Butyldimethylsilyloxy-2exo-chloro-7,7-diphenylbicyclo<3.2.0>heptan-6-one

Base Information

Chemical Name:3endo-t-Butyldimethylsilyloxy-2exo-chloro-7,7-diphenylbicyclo<3.2.0>heptan-6-one
CAS No.:125261-49-6
Molecular Formula:C₂₅H₃₁ClO₂Si
Molecular Weight:427.058
Hs Code.:

Synonyms:3endo-t-Butyldimethylsilyloxy-2exo-chloro-7,7-diphenylbicyclo<3.2.0>heptan-6-one

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Chemical Property of 3endo-t-Butyldimethylsilyloxy-2exo-chloro-7,7-diphenylbicyclo<3.2.0>heptan-6-one

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Technology Process of 3endo-t-Butyldimethylsilyloxy-2exo-chloro-7,7-diphenylbicyclo<3.2.0>heptan-6-one

There total 4 articles about 3endo-t-Butyldimethylsilyloxy-2exo-chloro-7,7-diphenylbicyclo<3.2.0>heptan-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 125261-43-0
6-t-Butyldimethylsilyloxy-3,3-diphenyltricyclo<3.2.0.0^1,4>heptan-2-one

: 125261-49-6
3endo-t-Butyldimethylsilyloxy-2exo-chloro-7,7-diphenylbicyclo<3.2.0>heptan-6-one

Guidance literature:: With ammonium chloride; water; iron; In methanol; diethyl ether; for 3h; Ambient temperature;
DOI:10.1039/P19900001353

Reference yield: 93.0%

: (1S,4S,5S,6S)-6-(tert-Butyl-dimethyl-silanyloxy)-3,3-diphenyl-tricyclo[3.2.0.0^1,4]heptan-2-one

: 125261-49-6
3endo-t-Butyldimethylsilyloxy-2exo-chloro-7,7-diphenylbicyclo<3.2.0>heptan-6-one

Guidance literature:: With iron; ammonium chloride; In methanol; for 4h; Ambient temperature;
DOI:10.1039/c39890000670

Reference yield:

: 125261-39-4
2exo-Bromo-3endo-t-butyldimethylsilyloxy-7,7-diphenylbicyclo<3.2.0>heptan-6-one

: 125261-49-6
3endo-t-Butyldimethylsilyloxy-2exo-chloro-7,7-diphenylbicyclo<3.2.0>heptan-6-one

Guidance literature:: Multi-step reaction with 2 steps

1: potassium t-butoxide

2: 93 percent / NH₄Cl, Fe / methanol / 4 h / Ambient temperature

With potassium tert-butylate; iron; ammonium chloride; In methanol;
DOI:10.1039/c39890000670