N-formyl-α-aminoisobutyric acid phenyl ester

Base Information

Chemical Name:N-formyl-α-aminoisobutyric acid phenyl ester
CAS No.:133859-55-9
Molecular Formula:C₁₁H₁₃NO₃
Molecular Weight:207.229
Hs Code.:

Synonyms:N-formyl-α-aminoisobutyric acid phenyl ester

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Chemical Property of N-formyl-α-aminoisobutyric acid phenyl ester

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Technology Process of N-formyl-α-aminoisobutyric acid phenyl ester

There total 1 articles about N-formyl-α-aminoisobutyric acid phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60421-25-2
N-formyl-2-aminoisobutyric acid

: 108-95-2,27073-41-2
phenol

: 133859-55-9
N-formyl-α-aminoisobutyric acid phenyl ester

Guidance literature:: With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In dichloromethane; for 3h; Yield given; Ambient temperature;
DOI:10.1021/ja983017e

Reference yield:

: {(η5-C5Me5)Rh(SCN)2}2

: 133859-55-9
N-formyl-α-aminoisobutyric acid phenyl ester

: {(η5-C5Me5)Rh(SCN)2(CNC(CH3)2CO2C6H5)}

Guidance literature:: With sodium hydrogencarbonate; triethylamine; trichlorophosphate; In dichloromethane; water; under N2 at -5°C, ester treated with (C2H5)3N soln. (CH2Cl2), POCl3 soln. (CH2Cl2), after 1 h warmed up, stirred for 18 h, treated with aq. NaHCO3, dilution and extn. with CH2Cl2, freeze-dried, treated with Rh complex, concn. after 3 h; plate chromy. (CH2Cl2/MeOH 19:1), elution of orange band with THF, evapn., chromy., elem. anal.;