C₂₄H₂₁NO₃S

Base Information

Chemical Name:C₂₄H₂₁NO₃S
CAS No.:1311293-14-7
Molecular Formula:C₂₄H₂₁NO₃S
Molecular Weight:403.502
Hs Code.:

C<sub>24</sub>H<sub>21</sub>NO<sub>3</sub>S

Synonyms:C₂₄H₂₁NO₃S

Suppliers and Price of C₂₄H₂₁NO₃S

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₄H₂₁NO₃S

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₄H₂₁NO₃S

There total 10 articles about C₂₄H₂₁NO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1311293-13-6
C₁₈H₁₅NO₃

: 108-98-5
thiophenol

: 1311293-14-7
C₂₄H₂₁NO₃S

Guidance literature:: With potassium carbonate; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.bmc.2011.03.024

Reference yield:

: 457071-58-8
4-{2-[3-(tetrahydro-pyran-2-yloxy)-prop-1-ynyl]-phenyl}-but-3-yn-1-ol

: 1311293-14-7
C₂₄H₂₁NO₃S

Guidance literature:: Multi-step reaction with 8 steps

1: triethylamine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

2: sodium azide / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

3: water; triphenylphosphine / tetrahydrofuran / Inert atmosphere

4: triethylamine / dichloromethane / 0.5 h / -10 - 0 °C / Inert atmosphere

5: pyridinium p-toluenesulfonate / ethanol / 2 h / 50 °C / Inert atmosphere

6: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere

7: acetic acid; triethylamine / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

8: potassium carbonate / dichloromethane / 2 h / 20 °C / Inert atmosphere

With sodium azide; water; pyridinium p-toluenesulfonate; potassium carbonate; Dess-Martin periodane; acetic acid; triethylamine; triphenylphosphine; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; 7: Knoevenagel condensation / 8: Michael addition;
DOI:10.1016/j.bmc.2011.03.024

Reference yield:

: 1311293-10-3
C₂₃H₂₇NO₅

: 1311293-14-7
C₂₄H₂₁NO₃S

Guidance literature:: Multi-step reaction with 4 steps

1: pyridinium p-toluenesulfonate / ethanol / 2 h / 50 °C / Inert atmosphere

2: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere

3: acetic acid; triethylamine / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

4: potassium carbonate / dichloromethane / 2 h / 20 °C / Inert atmosphere

With pyridinium p-toluenesulfonate; potassium carbonate; Dess-Martin periodane; acetic acid; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; 3: Knoevenagel condensation / 4: Michael addition;
DOI:10.1016/j.bmc.2011.03.024