C₁₆H₁₅BrN₂O₄

Base Information

Chemical Name:C₁₆H₁₅BrN₂O₄
CAS No.:1590410-12-0
Molecular Formula:C₁₆H₁₅BrN₂O₄
Molecular Weight:379.21
Hs Code.:

C<sub>16</sub>H<sub>15</sub>BrN<sub>2</sub>O<sub>4</sub>

Synonyms:C₁₆H₁₅BrN₂O₄

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Chemical Property of C₁₆H₁₅BrN₂O₄

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Technology Process of C₁₆H₁₅BrN₂O₄

There total 7 articles about C₁₆H₁₅BrN₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1590410-08-4
C₈H₇BrN₂O₃

: 824-94-2
p-methoxybenzyl chloride

: 1590410-12-0
C₁₆H₁₅BrN₂O₄

Guidance literature:: C₈H₇BrN₂O₃; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.5h;

p-methoxybenzyl chloride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 16h;

Reference yield:

: 629655-23-8
2-chloro-3-nitro-4-hydroxypyridine

: 1590410-12-0
C₁₆H₁₅BrN₂O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: N,N-dimethyl-formamide / 10 h / 80 °C

2.1: bromine / water / 1.5 h / 20 - 50 °C

3.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 16 h / 0 - 20 °C / Inert atmosphere

4.1: acetic acid; iron / 3 h / 80 °C

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C

5.2: 16 h / 20 °C

With di-isopropyl azodicarboxylate; bromine; iron; sodium hydride; acetic acid; triphenylphosphine; In tetrahydrofuran; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1590410-07-3
C₁₀H₁₁BrN₂O₆

: 1590410-12-0
C₁₆H₁₅BrN₂O₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid; iron / 3 h / 80 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C

2.2: 16 h / 20 °C

With iron; sodium hydride; acetic acid; In N,N-dimethyl-formamide; mineral oil;