Technology Process of 4-tert-butoxyphenylacetyl fluoride
There total 3 articles about 4-tert-butoxyphenylacetyl fluoride which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine; trifluoro-[1,3,5]triazine;
In
acetonitrile;
for 2h;
Ambient temperature;
DOI:10.1021/jm00068a008
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 96 percent / trifluoromethanesulfonic acid / CH2Cl2 / 1.) -78 deg C, 15 min, 2.) -20 deg C 45 min
2: 97 percent / aq. 1N NaOH / dioxane / 3 h / Ambient temperature
3: 99 percent / pyridine, cyanuric fluoride / acetonitrile / 2 h / Ambient temperature
With
pyridine; sodium hydroxide; trifluoro-[1,3,5]triazine; trifluorormethanesulfonic acid;
In
1,4-dioxane; dichloromethane; acetonitrile;
DOI:10.1021/jm00068a008
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 97 percent / aq. 1N NaOH / dioxane / 3 h / Ambient temperature
2: 99 percent / pyridine, cyanuric fluoride / acetonitrile / 2 h / Ambient temperature
With
pyridine; sodium hydroxide; trifluoro-[1,3,5]triazine;
In
1,4-dioxane; acetonitrile;
DOI:10.1021/jm00068a008
