(1R)-1-amino-2-(4-methoxyphenyl)-ethylboronic acid (+)-pinanediol ester trifluoroacetate

Base Information

Chemical Name:(1R)-1-amino-2-(4-methoxyphenyl)-ethylboronic acid (+)-pinanediol ester trifluoroacetate
CAS No.:1158974-86-7
Molecular Formula:C₂HF₃O₂*C₁₉H₂₈BNO₃
Molecular Weight:443.271
Hs Code.:

Synonyms:(1R)-1-amino-2-(4-methoxyphenyl)-ethylboronic acid (+)-pinanediol ester trifluoroacetate

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Chemical Property of (1R)-1-amino-2-(4-methoxyphenyl)-ethylboronic acid (+)-pinanediol ester trifluoroacetate

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Technology Process of (1R)-1-amino-2-(4-methoxyphenyl)-ethylboronic acid (+)-pinanediol ester trifluoroacetate

There total 1 articles about (1R)-1-amino-2-(4-methoxyphenyl)-ethylboronic acid (+)-pinanediol ester trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1158974-84-5
N-((R)-2-(4-methoxyphenyl)-1-((3aS,4S,6S,7aR)-3a,5,5-trimethylhexahydro-4,6-methanobenzo[d][1,3,2]dioxaborol-2-yl)ethyl)-1,1,1-trimethyl-N-(trimethylsilyl)silanamine

: 76-05-1
trifluoroacetic acid

: 1158974-86-7
(1R)-1-amino-2-(4-methoxyphenyl)-ethylboronic acid (+)-pinanediol ester trifluoroacetate

Guidance literature:: at 0 ℃; for 1h;
DOI:10.1016/j.bmcl.2009.02.117

Reference yield: 69.0%

: 1158974-97-0
Boc-Tyr(Me)-Val-OH

: 1158974-86-7
(1R)-1-amino-2-(4-methoxyphenyl)-ethylboronic acid (+)-pinanediol ester trifluoroacetate

: 1158974-98-1
(1R)-1-(N-tert-butoxycarbonyl-L-O-methyltyrosyl-L-valyl)amino-2-(4-methoxyphenyl)ethylboronic acid (+)-pinanediol ester

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 20h;
DOI:10.1016/j.bmcl.2009.02.117