carbonic acid-(3R,4S,5S,6R)-5-methoxy-4-[(2R,3R)-2-methyl-3-(3-methyl-but-2-enyl)-oxiranyl]-1-oxaspiro[2.5]oct-6-yl ester 4-nitro-phenyl ester

Base Information

Chemical Name:carbonic acid-(3R,4S,5S,6R)-5-methoxy-4-[(2R,3R)-2-methyl-3-(3-methyl-but-2-enyl)-oxiranyl]-1-oxaspiro[2.5]oct-6-yl ester 4-nitro-phenyl ester
CAS No.:1160640-95-8
Molecular Formula:C₂₃H₂₉NO₈
Molecular Weight:447.485
Hs Code.:

Synonyms:carbonic acid-(3R,4S,5S,6R)-5-methoxy-4-[(2R,3R)-2-methyl-3-(3-methyl-but-2-enyl)-oxiranyl]-1-oxaspiro[2.5]oct-6-yl ester 4-nitro-phenyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of carbonic acid-(3R,4S,5S,6R)-5-methoxy-4-[(2R,3R)-2-methyl-3-(3-methyl-but-2-enyl)-oxiranyl]-1-oxaspiro[2.5]oct-6-yl ester 4-nitro-phenyl ester

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

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Technology Process of carbonic acid-(3R,4S,5S,6R)-5-methoxy-4-[(2R,3R)-2-methyl-3-(3-methyl-but-2-enyl)-oxiranyl]-1-oxaspiro[2.5]oct-6-yl ester 4-nitro-phenyl ester

There total 3 articles about carbonic acid-(3R,4S,5S,6R)-5-methoxy-4-[(2R,3R)-2-methyl-3-(3-methyl-but-2-enyl)-oxiranyl]-1-oxaspiro[2.5]oct-6-yl ester 4-nitro-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 7693-46-1
4-Nitrophenyl chloroformate

: 35903-52-7,128656-25-7,132746-73-7,108102-51-8
fumagillol

: 1160640-95-8
carbonic acid-(3R,4S,5S,6R)-5-methoxy-4-[(2R,3R)-2-methyl-3-(3-methyl-but-2-enyl)-oxiranyl]-1-oxaspiro[2.5]oct-6-yl ester 4-nitro-phenyl ester

Guidance literature:: With triethylamine; In dichloromethane; for 8h; Inert atmosphere; Reflux;
DOI:10.1016/j.ejmech.2013.10.033

Reference yield:

: 5070-13-3
bis-(p-nitrophenyl) carbonate

: 35903-52-7,128656-25-7,132746-73-7,108102-51-8
fumagillol

: 1160640-95-8
carbonic acid-(3R,4S,5S,6R)-5-methoxy-4-[(2R,3R)-2-methyl-3-(3-methyl-but-2-enyl)-oxiranyl]-1-oxaspiro[2.5]oct-6-yl ester 4-nitro-phenyl ester

Guidance literature:: With dmap; In dichloromethane;

Reference yield:

: 41567-78-6
dicyclohexylamine (2E,4E,6E,8E)-10-(((3R,4S,5S,6R)-5-methoxy-4-((2R,3R)-2-methyl-3-(3-methylbut-2-en-1-yl)oxiran-2-yl)-1-oxaspiro[2.5]octan-6-yl)oxy)-10-oxodeca-2,4,6,8-tetraenoate

: 1160640-95-8
carbonic acid-(3R,4S,5S,6R)-5-methoxy-4-[(2R,3R)-2-methyl-3-(3-methyl-but-2-enyl)-oxiranyl]-1-oxaspiro[2.5]oct-6-yl ester 4-nitro-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; water / 3 h / 20 °C

2: dmap / dichloromethane / 0 - 20 °C

With water; sodium hydroxide; dmap; In dichloromethane;