N₄-(1,1-dimethylethyloxycarbonyl)-N₂-[2-[1-[(4-chlorophenyl)methyl]-1H-imidazol-5-yl]ethyl]-1,2(R)-piperazinecarboxamide

Base Information

• Chemical Name: N₄-(1,1-dimethylethyloxycarbonyl)-N₂-[2-[1-[(4-chlorophenyl)methyl]-1H-imidazol-5-yl]ethyl]-1,2(R)-piperazinecarboxamide
• CAS No.: 279237-41-1
• Molecular Formula: C₂₂H₃₀ClN₅O₃
• Molecular Weight: 447.965

Synonyms:N₄-(1,1-dimethylethyloxycarbonyl)-N₂-[2-[1-[(4-chlorophenyl)methyl]-1H-imidazol-5-yl]ethyl]-1,2(R)-piperazinecarboxamide

Chemical Property of N₄-(1,1-dimethylethyloxycarbonyl)-N₂-[2-[1-[(4-chlorophenyl)methyl]-1H-imidazol-5-yl]ethyl]-1,2(R)-piperazinecarboxamide

Chemical Property:

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Technology Process of N₄-(1,1-dimethylethyloxycarbonyl)-N₂-[2-[1-[(4-chlorophenyl)methyl]-1H-imidazol-5-yl]ethyl]-1,2(R)-piperazinecarboxamide

There total 2 articles about N₄-(1,1-dimethylethyloxycarbonyl)-N₂-[2-[1-[(4-chlorophenyl)methyl]-1H-imidazol-5-yl]ethyl]-1,2(R)-piperazinecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-Boc-piperazine-2-amidoanhydride (173774-50-0) + N-[(4-chlorophenyl)methyl]-histamine (279238-28-7) → N4-(1,1-dimethylethyloxycarbonyl)-N2-[2-[1-[(4-chlorophenyl)methyl]-1H-imidazol-5-yl]ethyl]-1,2(R)-piperazinecarboxamide (279237-41-1)

Guidance literature:

In dichloromethane; at 20 ℃;

Reference yield:

→ N4-(1,1-dimethylethyloxycarbonyl)-N2-[2-[1-[(4-chlorophenyl)methyl]-1H-imidazol-5-yl]ethyl]-1,2(R)-piperazinecarboxamide (279237-41-1)

Guidance literature:

Reference yield:

N4-(1,1-dimethylethyloxycarbonyl)-N2-[2-[1-[(4-chlorophenyl)methyl]-1H-imidazol-5-yl]ethyl]-1,2(R)-piperazinecarboxamide (279237-41-1) + Cyclohexyl isocyanate (3173-53-3) → N2-[2-[1-[(4-chlorophenyl)methyl]-1H-imidazol-5-yl]ethyl]-N1-cyclohexyl-1,2(R)-piperazinecarboxamide (279238-48-1)

Guidance literature:

N₄-(1,1-dimethylethyloxycarbonyl)-N₂-[2-[1-[(4-chlorophenyl)methyl]-1H-imidazol-5-yl]ethyl]-1,2(R)-piperazinecarboxamide; Cyclohexyl isocyanate; In dichloromethane; at 20 ℃; for 0.5h;

With trifluoroacetic acid; In dichloromethane; at 20 ℃;

upstream raw materials:

N-Boc-piperazine-2-amidoanhydride

N-[(4-chlorophenyl)methyl]-histamine

Downstream raw materials:

N₂-[2-[1-[(4-chlorophenyl)methyl]-1H-imidazol-5-yl]ethyl]-N₁-cyclohexyl-1,2(R)-piperazinecarboxamide

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