2,3,4-tri-O-benzoyl-6-S-phenyl-6-thio-α-D-galactopyranosyl trichloroacetimidate

Base Information

Chemical Name:2,3,4-tri-O-benzoyl-6-S-phenyl-6-thio-α-D-galactopyranosyl trichloroacetimidate
CAS No.:402730-85-2
Molecular Formula:C₃₅H₂₈Cl₃NO₈S
Molecular Weight:729.034
Hs Code.:

Synonyms:2,3,4-tri-O-benzoyl-6-S-phenyl-6-thio-α-D-galactopyranosyl trichloroacetimidate

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Chemical Property of 2,3,4-tri-O-benzoyl-6-S-phenyl-6-thio-α-D-galactopyranosyl trichloroacetimidate

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Technology Process of 2,3,4-tri-O-benzoyl-6-S-phenyl-6-thio-α-D-galactopyranosyl trichloroacetimidate

There total 5 articles about 2,3,4-tri-O-benzoyl-6-S-phenyl-6-thio-α-D-galactopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 545-06-2
trichloroacetonitrile

: C₃₃H₂₈O₈S

: 402730-85-2
2,3,4-tri-O-benzoyl-6-S-phenyl-6-thio-α-D-galactopyranosyl trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃;
DOI:10.1016/S0040-4020(01)00959-0

Reference yield:

: 104495-07-0
1,2:3,4-di-O-isopropylidene-6-S-phenyl-6-thio-α-D-galactopyranoside

: 402730-85-2
2,3,4-tri-O-benzoyl-6-S-phenyl-6-thio-α-D-galactopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 3 steps

1.1: aq. acetic acid / 5 h / 50 °C

1.2: 73 percent / pyridine / 20 °C

2.1: NH₃ / methanol; tetrahydrofuran / 0 °C

3.1: 1.37 g / DBU / CH₂Cl₂ / 20 °C

With ammonia; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/S0040-4020(01)00959-0

Reference yield:

: 882-33-7
diphenyldisulfane

: 402730-85-2
2,3,4-tri-O-benzoyl-6-S-phenyl-6-thio-α-D-galactopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 96 percent / tri-n-butylphosphine / pyridine / 24 h / 20 °C

2.1: aq. acetic acid / 5 h / 50 °C

2.2: 73 percent / pyridine / 20 °C

3.1: NH₃ / methanol; tetrahydrofuran / 0 °C

4.1: 1.37 g / DBU / CH₂Cl₂ / 20 °C

With tributylphosphine; ammonia; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; pyridine; methanol; dichloromethane;
DOI:10.1016/S0040-4020(01)00959-0