N-phenyl 2(R),6(R),7(S),8(R) 6-isopropyl-2-phenyl-1-aza-4-oxa<4.3.0^1,6>bicyclononan-5-one-7,8-dicarboximide

Base Information

• Chemical Name: N-phenyl 2(R),6(R),7(S),8(R) 6-isopropyl-2-phenyl-1-aza-4-oxa<4.3.0^1,6>bicyclononan-5-one-7,8-dicarboximide
• CAS No.: 138535-52-1
• Molecular Formula: C₂₄H₂₄N₂O₄
• Molecular Weight: 404.466

Synonyms:N-phenyl 2(R),6(R),7(S),8(R) 6-isopropyl-2-phenyl-1-aza-4-oxa<4.3.0^1,6>bicyclononan-5-one-7,8-dicarboximide

Chemical Property of N-phenyl 2(R),6(R),7(S),8(R) 6-isopropyl-2-phenyl-1-aza-4-oxa<4.3.0^1,6>bicyclononan-5-one-7,8-dicarboximide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

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Useful:

Technology Process of N-phenyl 2(R),6(R),7(S),8(R) 6-isopropyl-2-phenyl-1-aza-4-oxa<4.3.0^1,6>bicyclononan-5-one-7,8-dicarboximide

There total 2 articles about N-phenyl 2(R),6(R),7(S),8(R) 6-isopropyl-2-phenyl-1-aza-4-oxa<4.3.0^1,6>bicyclononan-5-one-7,8-dicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + N-phenyl-maleimide (941-69-5) + (3R,5R)-3-Isopropyl-5-phenyl-morpholin-2-one (64975-86-6) → N-phenyl 2(R),6(R),7(R),8(S) 6-isopropyl-2-phenyl-1-aza-4-oxa<4.3.01,6>bicyclononan-5-one-7,8-dicarboximide (138604-89-4) + N-phenyl 2(R),6(R),7(S),8(R) 6-isopropyl-2-phenyl-1-aza-4-oxa<4.3.01,6>bicyclononan-5-one-7,8-dicarboximide (138535-52-1)

Guidance literature:

With molecular sieve; In toluene; Heating;

DOI:10.1016/S0957-4166(00)86146-7

Reference yield: 34.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + N-phenyl-maleimide (941-69-5) + 3(S)-isopropyl-5(S)-phenylmorpholine (64975-86-6) → N-phenyl 2(R),6(R),7(R),8(S) 6-isopropyl-2-phenyl-1-aza-4-oxa<4.3.01,6>bicyclononan-5-one-7,8-dicarboximide (138604-89-4) + N-phenyl 2(R),6(R),7(S),8(R) 6-isopropyl-2-phenyl-1-aza-4-oxa<4.3.01,6>bicyclononan-5-one-7,8-dicarboximide (138535-52-1)

Guidance literature:

With 3 A molecular sieve; In toluene; for 2h; Heating;

DOI:10.1016/S0957-4166(00)80031-2

Reference yield: 72.0%

N-phenyl 2(R),6(R),7(S),8(R) 6-isopropyl-2-phenyl-1-aza-4-oxa<4.3.01,6>bicyclononan-5-one-7,8-dicarboximide (138535-52-1) → 2(R),3(S),4(R) 2-isopropyl-3,4-(N-phenyl dicarboximido)pyrrolidine-2-carboxylic acid (138535-55-4)

Guidance literature:

With hydrogen; trifluoroacetic acid; palladium dihydroxide; In methanol; Ambient temperature;

DOI:10.1016/S0957-4166(00)86146-7

upstream raw materials:

formaldehyd

N-phenyl-maleimide

(3R,5R)-3-Isopropyl-5-phenyl-morpholin-2-one

3(S)-isopropyl-5(S)-phenylmorpholine

Downstream raw materials:

2(R),3(S),4(R) 2-isopropyl-3,4-(N-phenyl dicarboximido)pyrrolidine-2-carboxylic acid

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