6-(4,6-diphenylpyrimidin-2-yl)-12,12-dimethyl-2-phenyl-6,12-dihydro-6-azaindeno[1,2-b]fluorene

Base Information

Chemical Name:6-(4,6-diphenylpyrimidin-2-yl)-12,12-dimethyl-2-phenyl-6,12-dihydro-6-azaindeno[1,2-b]fluorene
CAS No.:1307286-01-6
Molecular Formula:C₄₃H₃₁N₃
Molecular Weight:589.739
Hs Code.:

Synonyms:6-(4,6-diphenylpyrimidin-2-yl)-12,12-dimethyl-2-phenyl-6,12-dihydro-6-azaindeno[1,2-b]fluorene

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Chemical Property of 6-(4,6-diphenylpyrimidin-2-yl)-12,12-dimethyl-2-phenyl-6,12-dihydro-6-azaindeno[1,2-b]fluorene

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Technology Process of 6-(4,6-diphenylpyrimidin-2-yl)-12,12-dimethyl-2-phenyl-6,12-dihydro-6-azaindeno[1,2-b]fluorene

There total 6 articles about 6-(4,6-diphenylpyrimidin-2-yl)-12,12-dimethyl-2-phenyl-6,12-dihydro-6-azaindeno[1,2-b]fluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 1307286-00-5
12,12-dimethyl-2-phenyl-6,12-dihydro-6-azaindeno[1,2-b]fluorene

: 2915-16-4
2-chloro-4,6-diphenylpyrimidine

: 1307286-01-6
6-(4,6-diphenylpyrimidin-2-yl)-12,12-dimethyl-2-phenyl-6,12-dihydro-6-azaindeno[1,2-b]fluorene

Guidance literature:: 12,12-dimethyl-2-phenyl-6,12-dihydro-6-azaindeno[1,2-b]fluorene; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 1h; Inert atmosphere;

2-chloro-4,6-diphenylpyrimidine; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 12h;

Reference yield:

: 98-80-6
phenylboronic acid

: 1307286-01-6
6-(4,6-diphenylpyrimidin-2-yl)-12,12-dimethyl-2-phenyl-6,12-dihydro-6-azaindeno[1,2-b]fluorene

Guidance literature:: Multi-step reaction with 2 steps

1.1: tris-(o-tolyl)phosphine; palladium diacetate; sodium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / Reflux

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 20 °C / Inert atmosphere

2.2: 12 h / 20 °C

With palladium diacetate; sodium hydride; sodium hydrogencarbonate; tris-(o-tolyl)phosphine; In 1,2-dimethoxyethane; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1307285-98-8
7-bromo-2-(2-nitrophenyl)-9,9-dimethyl-9H-fluorene

: 1307286-01-6
6-(4,6-diphenylpyrimidin-2-yl)-12,12-dimethyl-2-phenyl-6,12-dihydro-6-azaindeno[1,2-b]fluorene

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethyl phosphite / 12 h / Reflux

2.1: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 16 h / Reflux

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 20 °C / Inert atmosphere

3.2: 12 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydride; sodium carbonate; triethyl phosphite; In N,N-dimethyl-formamide; mineral oil;