2-amino-5-iodoisophthalic acid

Base Information

Chemical Name:2-amino-5-iodoisophthalic acid
CAS No.:907574-30-5
Molecular Formula:C₈H₆INO₄
Molecular Weight:307.044
Hs Code.:

Synonyms:2-amino-5-iodoisophthalic acid

Suppliers and Price of 2-amino-5-iodoisophthalic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Matrix Scientific
2-Amino-5-iodoisophthalic acid 95%
5g
$ 1666.00

Matrix Scientific
2-Amino-5-iodoisophthalic acid 95%
1g
$ 1110.00

Total 0 raw suppliers

Chemical Property of 2-amino-5-iodoisophthalic acid

Chemical Property:

Purity/Quality:: 2-Amino-5-iodoisophthalic acid 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-amino-5-iodoisophthalic acid

There total 1 articles about 2-amino-5-iodoisophthalic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39622-79-2
2-aminoisophthalic acid

: 907574-30-5
2-amino-5-iodoisophthalic acid

Guidance literature:: With Iodine monochloride; In acetic acid; at 20 ℃; for 2.25h;

Reference yield:

: 907574-30-5
2-amino-5-iodoisophthalic acid

: 18595-18-1
3-amino-4-methyl benzoic acid methyl ester

: 907574-31-6
6-iodo-3-[5-(methoxycarbonyl)-2-methylphenyl]-4-oxo-3,4-dihydroquinazoline-8-carboxylic acid

Guidance literature:: 2-amino-5-iodoisophthalic acid; orthoformic acid triethyl ester; With acetic acid; In toluene; at 100 ℃; for 25h;

3-amino-4-methyl benzoic acid methyl ester; In toluene; at 100 ℃; for 21h;

Reference yield:

: 907574-30-5
2-amino-5-iodoisophthalic acid

: 1269420-62-3
4-amino-6-(3-hydroxy-prop-1-ynyl)-quinazoline-8-carboxylic acid [2,6-difluoro-3-(propane-1-sulfonyl-amino)phenyl]amide

Guidance literature:: Multi-step reaction with 7 steps

1.1: 0.25 h / 170 - 185 °C

2.1: sulfuric acid / 32 h / Reflux

3.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0.5 h

3.2: 48 h / 20 °C

4.1: triethylamine / copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

5.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 4 h / 65 °C

5.2: pH 5 / Acidic conditions

6.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 16 h / 20 °C

7.1: trifluoroacetic acid / 1 h / 85 °C

With lithium hydroxide monohydrate; sulfuric acid; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;