4-O-benzyl-5,6-O-(cyclohexane-1,1-diyl)-2,3-dideoxy-1-O-(4-methoxybenzyl)-d-erythrohexitol

Base Information

Chemical Name:4-O-benzyl-5,6-O-(cyclohexane-1,1-diyl)-2,3-dideoxy-1-O-(4-methoxybenzyl)-d-erythrohexitol
CAS No.:1401872-11-4
Molecular Formula:C₂₇H₃₆O₅
Molecular Weight:440.58
Hs Code.:

Synonyms:4-O-benzyl-5,6-O-(cyclohexane-1,1-diyl)-2,3-dideoxy-1-O-(4-methoxybenzyl)-d-erythrohexitol

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Chemical Property of 4-O-benzyl-5,6-O-(cyclohexane-1,1-diyl)-2,3-dideoxy-1-O-(4-methoxybenzyl)-d-erythrohexitol

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Technology Process of 4-O-benzyl-5,6-O-(cyclohexane-1,1-diyl)-2,3-dideoxy-1-O-(4-methoxybenzyl)-d-erythrohexitol

There total 2 articles about 4-O-benzyl-5,6-O-(cyclohexane-1,1-diyl)-2,3-dideoxy-1-O-(4-methoxybenzyl)-d-erythrohexitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1380510-77-9
C₁₉H₂₈O₄

: 2746-25-0
p-Methoxybenzyl bromide

: 1401872-11-4
4-O-benzyl-5,6-O-(cyclohexane-1,1-diyl)-2,3-dideoxy-1-O-(4-methoxybenzyl)-d-erythrohexitol

Guidance literature:: C₁₉H₂₈O₄; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;

p-Methoxybenzyl bromide; In tetrahydrofuran; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1002/hlca.201200064

Reference yield:

: 942137-19-1
(2R)-2-[(1S)-1-(benzyloxy)-3-butenyl]-1,4-dioxaspiro[4.5]decane

: 1401872-11-4
4-O-benzyl-5,6-O-(cyclohexane-1,1-diyl)-2,3-dideoxy-1-O-(4-methoxybenzyl)-d-erythrohexitol

Guidance literature:: Multi-step reaction with 2 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran; cyclohexene / 3 h / 0 °C / Inert atmosphere

1.2: 2 h / 0 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

2.2: 6 h / 20 °C / Inert atmosphere

With dimethylsulfide borane complex; sodium hydride; In tetrahydrofuran; cyclohexene;
DOI:10.1002/hlca.201200064