2-Diazo-succinic acid 4-tert-butyl ester 1-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester

Base Information

Chemical Name:2-Diazo-succinic acid 4-tert-butyl ester 1-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester
CAS No.:158393-63-6
Molecular Formula:C₁₈H₃₀N₂O₄
Molecular Weight:338.447
Hs Code.:

Synonyms:2-Diazo-succinic acid 4-tert-butyl ester 1-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester

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Chemical Property of 2-Diazo-succinic acid 4-tert-butyl ester 1-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester

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Technology Process of 2-Diazo-succinic acid 4-tert-butyl ester 1-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester

There total 3 articles about 2-Diazo-succinic acid 4-tert-butyl ester 1-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2216-51-5
(-)-menthol

: 158393-63-6
2-Diazo-succinic acid 4-tert-butyl ester 1-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / NaOAc / acetonitrile / 2 h / Heating

2: 1.) NaH, 2.) NEt₃, MsN₃ / 1.) THF, 0 deg C, 30 min; room temperature, 12 h, 2.) CH₃CN, room temperature, 4 d

With sodium acetate; sodium hydride; triethylamine; Methanesulfonyl azide; In acetonitrile;
DOI:10.1016/S0040-4020(97)00002-1

Reference yield:

: 2216-51-5
(-)-menthol

: 158393-63-6
2-Diazo-succinic acid 4-tert-butyl ester 1-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: NaOAc / acetonitrile / Heating

2: 1.) NaH, 2.) MsN₃, NEt₃ / 2.) RT, 96 h

With sodium acetate; sodium hydride; triethylamine; Methanesulfonyl azide; In acetonitrile;
DOI:10.1016/S0040-4039(00)60729-3

Reference yield:

: 59557-05-0
(L)-menthyl 3-oxobutyrate

: 158393-63-6
2-Diazo-succinic acid 4-tert-butyl ester 1-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester

Guidance literature:: With sodium hydride; triethylamine; Methanesulfonyl azide; Yield given. Multistep reaction; 2.) RT, 96 h;
DOI:10.1016/S0040-4039(00)60729-3