N-tert-butyl-N-phenylhydrazine

Base Information

• Chemical Name: N-tert-butyl-N-phenylhydrazine
• CAS No.: 36171-18-3
• Molecular Formula: C₁₀H₁₆N₂
• Molecular Weight: 164.25
• Mol file: 36171-18-3.mol

Synonyms:N-tert-butyl-N-phenylhydrazine

Chemical Property of N-tert-butyl-N-phenylhydrazine

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-tert-butyl-N-phenylhydrazine

There total 2 articles about N-tert-butyl-N-phenylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

N-tert-butyl-N-phenylnitrosamine (24642-84-0) → N-tert-butyl-N-phenylhydrazine (36171-18-3)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 16h; Heating;

DOI:10.1021/jo00326a006

Reference yield:

→ N-tert-butyl-N-phenylhydrazine (36171-18-3)

Guidance literature:

entspr. N-Nitroso-anilin 6, Reduktion;

DOI:10.1021/ja00760a029

Reference yield: 78.0%

N-tert-butyl-N-phenylhydrazine (36171-18-3) → tert-butyl methyl ether (1634-04-4) + N-tert-butylaniline (937-33-7) + Phenyl azide (622-37-7)

Guidance literature:

With tetrafluoroboric acid; isopentyl nitrite; In methanol; at 50 ℃; for 20h; under 0.5 - 1 Torr; Product distribution; Mechanism; dependence of product distribution on solvent and acid;

DOI:10.1021/jo00326a006

upstream raw materials:

N-tert-butyl-N-phenylnitrosamine

Downstream raw materials:

tert-butyl methyl ether

N-tert-butylaniline

Phenyl azide

Refernces