4-tert-butoxycarbonylaminobutyric acid 2-(3-carbamoyl-4-hydroxyphenyl)-2-oxoethyl ester

Base Information

Chemical Name:4-tert-butoxycarbonylaminobutyric acid 2-(3-carbamoyl-4-hydroxyphenyl)-2-oxoethyl ester
CAS No.:1292299-11-6
Molecular Formula:C₁₈H₂₄N₂O₇
Molecular Weight:380.398
Hs Code.:

Synonyms:4-tert-butoxycarbonylaminobutyric acid 2-(3-carbamoyl-4-hydroxyphenyl)-2-oxoethyl ester

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Chemical Property of 4-tert-butoxycarbonylaminobutyric acid 2-(3-carbamoyl-4-hydroxyphenyl)-2-oxoethyl ester

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Technology Process of 4-tert-butoxycarbonylaminobutyric acid 2-(3-carbamoyl-4-hydroxyphenyl)-2-oxoethyl ester

There total 2 articles about 4-tert-butoxycarbonylaminobutyric acid 2-(3-carbamoyl-4-hydroxyphenyl)-2-oxoethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 57294-38-9
N-(tert-butoxycarbonyl)-4-aminobutanoic acid

: 73866-23-6
5-(2-bromoacetyl)-2-hydroxybenzamide

: 1292299-11-6
4-tert-butoxycarbonylaminobutyric acid 2-(3-carbamoyl-4-hydroxyphenyl)-2-oxoethyl ester

Guidance literature:: With potassium carbonate; In acetonitrile; at 20 ℃;
DOI:10.1139/V10-143

Reference yield:

: 40187-51-7
5-acetylsalicylamide

: 1292299-11-6
4-tert-butoxycarbonylaminobutyric acid 2-(3-carbamoyl-4-hydroxyphenyl)-2-oxoethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: phenyltrimethylammonium tribromide / methanol; dichloromethane / 20 °C

2: potassium carbonate / acetonitrile / 20 °C

With phenyltrimethylammonium tribromide; potassium carbonate; In methanol; dichloromethane; acetonitrile;
DOI:10.1139/V10-143