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5-Acetylsalicylamide Manufacturer/High quality/Best price/In stock
Cas No: 40187-51-7
USD $ 3.0-3.0 / Kilogram 1 Kilogram 1-100 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
High quality 5-Acetylsalicylamide
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No Data 1 Kilogram 30 Metric Ton/Month Simagchem Corporation Contact Supplier
5-Acetylsalicylamide
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No Data 1 Kilogram 20 Metric Ton/Week Henan Allgreen Chemical Co.,Ltd Contact Supplier
5-acetyl-2-hydroxybenzamide
Cas No: 40187-51-7
No Data 10 Milligram Amadis Chemical Co., Ltd. Contact Supplier
5-Acetylsalicylamide
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No Data No Data No Data Chemwill Asia Co., Ltd. Contact Supplier
5-Acetylsalicylamide
Cas No: 40187-51-7
USD $ 1.0-1.0 / Kilogram 1 Kilogram 1000 Metric Ton/Year Henan Sinotech Import&Export Corporation Contact Supplier
5-Acetylsalicylamide 40187-51-7 For Pharmaceutical Intermediates
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No Data 10 Gram 10000 Metric Ton/Month Hubei XinRunde Chemical Co., Ltd Contact Supplier
ProfessionalCAS 40187-51-7 with fast shipping
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USD $ 146.0-176.0 / Gram 10 Gram 1000 Kilogram/Day Zhuozhou Wenxi import and Export Co., Ltd Contact Supplier
BLOOM TECH Advanced API/Technology support 5-Acetyl-2-hydroxybenzamide CAS 40187-51-7
Cas No: 40187-51-7
No Data 1 Gram 3 Metric Ton/Month Shaanxi BLOOM TECH Co.,Ltd Contact Supplier
5-Acetylsalicylamide 40187-51-7
Cas No: 40187-51-7
No Data 1 Kilogram 10000 Metric Ton/Month Shanghai Upbio Tech Co.,Ltd Contact Supplier

40187-51-7 Usage

Chemical Properties

cream to beige powder
InChI:InChI=1/C9H9NO3/c1-5(11)6-2-3-8(12)7(4-6)9(10)13/h2-4,12H,1H3,(H2,10,13)

40187-51-7 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Alfa Aesar (A18303)  5-Acetylsalicylamide, 98%    40187-51-7 100g 1698.0CNY Detail
Alfa Aesar (A18303)  5-Acetylsalicylamide, 98%    40187-51-7 25g 532.0CNY Detail
Alfa Aesar (A18303)  5-Acetylsalicylamide, 98%    40187-51-7 5g 289.0CNY Detail

40187-51-7SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 11, 2017

Revision Date: Aug 11, 2017

1.Identification

1.1 GHS Product identifier

Product name 5-Acetyl-2-hydroxybenzamide

1.2 Other means of identification

Product number -
Other names 5-Acetylsalicylamide

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:40187-51-7 SDS

40187-51-7Synthetic route

acetyl chloride
75-36-5

acetyl chloride

salicylamide
65-45-2

salicylamide

5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

Conditions
ConditionsYield
With aluminum (III) chloride In nitromethane; dichloromethane at 0 - 20℃; Friedel-Crafts Acylation;95%
With aluminum (III) chloride; sodium chloride at 140℃; for 0.666667h; Temperature; Reagent/catalyst;92.2%
Stage #1: salicylamide With aluminum (III) chloride; sodium chloride In water at 180℃; for 3h;
Stage #2: acetyl chloride In water at 180℃; for 4h;
88.5%
With aluminium trichloride
O-acetylsalicylamide
5663-71-8

O-acetylsalicylamide

5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

Conditions
ConditionsYield
With aluminium trichloride
(3-Carbamoyl-4-hydroxy-benzyl)-carbamic acid tert-butyl ester

(3-Carbamoyl-4-hydroxy-benzyl)-carbamic acid tert-butyl ester

5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

(bromomethylcyclohexane)
2550-36-9

(bromomethylcyclohexane)

5-acetyl-2-(cyclohexylmethoxy)benzamide
189393-76-8

5-acetyl-2-(cyclohexylmethoxy)benzamide

Conditions
ConditionsYield
Stage #1: 5-acetylsalicylamide With caesium carbonate In methanol; water for 0.5h; Metallation;
Stage #2: Cyclohexylmethyl bromide In N,N-dimethyl-formamide at 90℃; for 42h; Alkylation;
98%
5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

benzyl bromide
100-39-0

benzyl bromide

5-acetyl-2-(phenylmethoxy)benzamide
75637-30-8

5-acetyl-2-(phenylmethoxy)benzamide

Conditions
ConditionsYield
With potassium carbonate In acetonitrile Reflux;98%
With potassium carbonate In acetonitrile Reflux;98%
With sodium methylate In methanol80%
5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

5-acetylbenzo[d]oxazol-2(3H)-one
54209-84-6

5-acetylbenzo[d]oxazol-2(3H)-one

Conditions
ConditionsYield
With [bis(acetoxy)iodo]benzene; potassium hydroxide In methanol at 0℃; for 1.08333h; Hofmann Rearrangement;89%
5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

4-fluorobenzaldehyde
459-57-4

4-fluorobenzaldehyde

(E)-5-(3-(4-fluorophenyl)acryloyl)-2-hydroxybenzamide

(E)-5-(3-(4-fluorophenyl)acryloyl)-2-hydroxybenzamide

Conditions
ConditionsYield
With thionyl chloride In ethanol at 25℃; for 14h;83%
With thionyl chloride In ethanol at 25℃; for 24h; Claisen-Schmidt Condensation;
5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

5-(2-bromoacetyl)-2-hydroxybenzamide
73866-23-6

5-(2-bromoacetyl)-2-hydroxybenzamide

Conditions
ConditionsYield
With hydrogen bromide; bromine In ethyl acetate at 5 - 10℃; for 18h;69.4%
With phenyltrimethylammonium tribromide In methanol; dichloromethane at 20℃;29%
Stage #1: 5-acetylsalicylamide With copper(I) bromide In ethyl acetate under 760.014 Torr; Inert atmosphere;
Stage #2: under 760.014 Torr;
5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

2,2-dimethoxy-propane
77-76-9

2,2-dimethoxy-propane

6-Acetyl-2,2-dimethyl-2,3-dihydro-benzo[e][1,3]oxazin-4-one
142167-24-6

6-Acetyl-2,2-dimethyl-2,3-dihydro-benzo[e][1,3]oxazin-4-one

Conditions
ConditionsYield
With toluene-4-sulfonic acid In acetone Heating;36%
5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

ethylene dibromide
106-93-4

ethylene dibromide

C11H12BrNO3

C11H12BrNO3

Conditions
ConditionsYield
With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate In ethyl acetate Reflux;35%
5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

benzyl chloride
100-44-7

benzyl chloride

5-acetyl-2-(phenylmethoxy)benzamide
75637-30-8

5-acetyl-2-(phenylmethoxy)benzamide

Conditions
ConditionsYield
With sodium methylate 1.) DMF, 2.) DMF, heating, 7 h; Yield given. Multistep reaction;
trifluoromethylsulfonic anhydride
358-23-6

trifluoromethylsulfonic anhydride

5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

trifluoro-methanesulfonic acid 4-acetyl-2-carbamoyl-phenyl ester

trifluoro-methanesulfonic acid 4-acetyl-2-carbamoyl-phenyl ester

Conditions
ConditionsYield
With triethylamine at -40℃;
5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

4-(2-furyl)-3-(carboxamido)phenyl-1-ethanone
343339-00-4

4-(2-furyl)-3-(carboxamido)phenyl-1-ethanone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Et3N / -40 °C
2: Pd(PPh3)4; LiCl / dioxane / 110 °C
View Scheme
5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

1-[4-(2-furyl)3-(carboxamido)phenyl]-4,4,4-trifluoro-1,3-butanedione
343339-01-5

1-[4-(2-furyl)3-(carboxamido)phenyl]-4,4,4-trifluoro-1,3-butanedione

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: Et3N / -40 °C
2: Pd(PPh3)4; LiCl / dioxane / 110 °C
3: NaOMe / 1,2-dimethoxy-ethane / 20 °C
View Scheme
5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

2-furan-2-yl-5-[2-(5-methanesulfonyl-pyridin-2-yl)-5-trifluoromethyl-2H-pyrazol-3-yl]-benzamide

2-furan-2-yl-5-[2-(5-methanesulfonyl-pyridin-2-yl)-5-trifluoromethyl-2H-pyrazol-3-yl]-benzamide

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: Et3N / -40 °C
2: Pd(PPh3)4; LiCl / dioxane / 110 °C
3: NaOMe / 1,2-dimethoxy-ethane / 20 °C
4: ethanol / Heating
View Scheme
5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

2-furan-2-yl-5-[1-(5-methanesulfonyl-pyridin-2-yl)-5-trifluoromethyl-1H-pyrazol-3-yl]-benzamide

2-furan-2-yl-5-[1-(5-methanesulfonyl-pyridin-2-yl)-5-trifluoromethyl-1H-pyrazol-3-yl]-benzamide

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: Et3N / -40 °C
2: Pd(PPh3)4; LiCl / dioxane / 110 °C
3: NaOMe / 1,2-dimethoxy-ethane / 20 °C
4: ethanol / Heating
View Scheme
5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

2-hydroxy-5-(1,3-thiazol-5-yl)-benzamide

2-hydroxy-5-(1,3-thiazol-5-yl)-benzamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 69.4 percent / HBr; bromine / ethyl acetate / 18 h / 5 - 10 °C
2: 36 percent / ethanol / 6 h / Heating
View Scheme
5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

2-hydroxy-5-(2-methyl-thiazol-5-yl)-benzamide
799280-24-3

2-hydroxy-5-(2-methyl-thiazol-5-yl)-benzamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 69.4 percent / HBr; bromine / ethyl acetate / 18 h / 5 - 10 °C
2: 75 percent / ethanol / 6 h / Heating
View Scheme
5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

5-(2-amino-thiazol-5-yl)-2-hydroxy-benzamide
799280-23-2

5-(2-amino-thiazol-5-yl)-2-hydroxy-benzamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 69.4 percent / HBr; bromine / ethyl acetate / 18 h / 5 - 10 °C
2: 65 percent / ethanol / 6 h / Heating
View Scheme
5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

2-hydroxy-5-(2-isopropyl-1,3-thiazol-5-yl)-benzamide

2-hydroxy-5-(2-isopropyl-1,3-thiazol-5-yl)-benzamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 69.4 percent / HBr; bromine / ethyl acetate / 18 h / 5 - 10 °C
2: 46 percent / ethanol / 6 h / Heating
View Scheme
5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

5-(2-methyl-thiazol-5-yl)-2-propoxy-benzamide

5-(2-methyl-thiazol-5-yl)-2-propoxy-benzamide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 69.4 percent / HBr; bromine / ethyl acetate / 18 h / 5 - 10 °C
2: 75 percent / ethanol / 6 h / Heating
3: 90 percent / potassium carbonate / dimethylformamide / 60 °C
View Scheme
5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

5-(2-amino-thiazol-5-yl)-2-propoxy-benzamide

5-(2-amino-thiazol-5-yl)-2-propoxy-benzamide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 69.4 percent / HBr; bromine / ethyl acetate / 18 h / 5 - 10 °C
2: 65 percent / ethanol / 6 h / Heating
3: 92 percent / potassium carbonate / dimethylformamide / 60 °C
View Scheme
5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

2-butoxy-5-(2-methyl-thiazol-5-yl)-benzamide

2-butoxy-5-(2-methyl-thiazol-5-yl)-benzamide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 69.4 percent / HBr; bromine / ethyl acetate / 18 h / 5 - 10 °C
2: 75 percent / ethanol / 6 h / Heating
3: 94 percent / potassium carbonate / dimethylformamide / 60 °C
View Scheme
5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

2-hydroxy-5-[2-(pyridin-2-ylamino)-thiazol-5-yl]-benzamide

2-hydroxy-5-[2-(pyridin-2-ylamino)-thiazol-5-yl]-benzamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 69.4 percent / HBr; bromine / ethyl acetate / 18 h / 5 - 10 °C
2: 57 percent / ethanol / 6 h / Heating
View Scheme
5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

2-hydroxy-5-(2-phenylamino-thiazol-5-yl)-benzamide
799280-05-0

2-hydroxy-5-(2-phenylamino-thiazol-5-yl)-benzamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 69.4 percent / HBr; bromine / ethyl acetate / 18 h / 5 - 10 °C
2: 65 percent / ethanol / 6 h / Heating
View Scheme
5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

2-hydroxy-5-(2-o-tolylamino-thiazol-5-yl)-benzamide

2-hydroxy-5-(2-o-tolylamino-thiazol-5-yl)-benzamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 69.4 percent / HBr; bromine / ethyl acetate / 18 h / 5 - 10 °C
2: 62 percent / ethanol / 6 h / Heating
View Scheme
5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

2-hydroxy-5-(2-p-tolylamino-thiazol-5-yl)-benzamide
799280-07-2

2-hydroxy-5-(2-p-tolylamino-thiazol-5-yl)-benzamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 69.4 percent / HBr; bromine / ethyl acetate / 18 h / 5 - 10 °C
2: 61 percent / ethanol / 6 h / Heating
View Scheme
5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

5-[2-(3-chloro-phenylamino)-thiazol-5-yl]-2-hydroxy-benzamide
799280-09-4

5-[2-(3-chloro-phenylamino)-thiazol-5-yl]-2-hydroxy-benzamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 69.4 percent / HBr; bromine / ethyl acetate / 18 h / 5 - 10 °C
2: 52 percent / ethanol / 6 h / Heating
View Scheme
5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

5-(2-phenylamino-thiazol-5-yl)-2-propoxy-benzamide

5-(2-phenylamino-thiazol-5-yl)-2-propoxy-benzamide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 69.4 percent / HBr; bromine / ethyl acetate / 18 h / 5 - 10 °C
2: 65 percent / ethanol / 6 h / Heating
3: 95 percent / potassium carbonate / dimethylformamide / 60 °C
View Scheme
5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

5-[2-(4-chloro-phenylamino)-thiazol-5-yl]-2-hydroxy-benzamide

5-[2-(4-chloro-phenylamino)-thiazol-5-yl]-2-hydroxy-benzamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 69.4 percent / HBr; bromine / ethyl acetate / 18 h / 5 - 10 °C
2: 49 percent / ethanol / 6 h / Heating
View Scheme
5-acetylsalicylamide
40187-51-7

5-acetylsalicylamide

2-hydroxy-5-[2-(6-methyl-pyridin-2-ylamino)-thiazol-5-yl]-benzamide

2-hydroxy-5-[2-(6-methyl-pyridin-2-ylamino)-thiazol-5-yl]-benzamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 69.4 percent / HBr; bromine / ethyl acetate / 18 h / 5 - 10 °C
2: 68 percent / ethanol / 6 h / Heating
View Scheme

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