3-Phenyl-8a-trimethylsilanyloxy-4a,5,6,7,8,8a-hexahydro-4H-benzo[e][1,2]oxazine

Base Information

• Chemical Name: 3-Phenyl-8a-trimethylsilanyloxy-4a,5,6,7,8,8a-hexahydro-4H-benzo[e][1,2]oxazine
• CAS No.: 109925-95-3
• Molecular Formula: C₁₇H₂₅NO₂Si
• Molecular Weight: 303.476

Synonyms:3-Phenyl-8a-trimethylsilanyloxy-4a,5,6,7,8,8a-hexahydro-4H-benzo[e][1,2]oxazine

Chemical Property of 3-Phenyl-8a-trimethylsilanyloxy-4a,5,6,7,8,8a-hexahydro-4H-benzo[e][1,2]oxazine

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Technology Process of 3-Phenyl-8a-trimethylsilanyloxy-4a,5,6,7,8,8a-hexahydro-4H-benzo[e][1,2]oxazine

There total 2 articles about 3-Phenyl-8a-trimethylsilanyloxy-4a,5,6,7,8,8a-hexahydro-4H-benzo[e][1,2]oxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

1-(Trimethylsilyloxy)cyclohexene (6651-36-1) + 2-chloro-1-phenyl-ethanone oxime (21572-32-7) → 3-Phenyl-8a-trimethylsilanyloxy-4a,5,6,7,8,8a-hexahydro-4H-benzo[e][1,2]oxazine (109925-95-3)

Guidance literature:

With sodium carbonate; In diethyl ether; for 120h; Ambient temperature;

DOI:10.1055/s-1987-27856

Reference yield: 49.0%

1-(Trimethylsilyloxy)cyclohexene (6651-36-1) + 2-bromo-1-phenyl-ethanone oxime (14181-72-7,17082-13-2,17082-14-3) → 3-Phenyl-8a-trimethylsilanyloxy-4a,5,6,7,8,8a-hexahydro-4H-benzo[e][1,2]oxazine (109925-95-3)

Guidance literature:

With sodium carbonate; In acetonitrile; for 20h; Ambient temperature;

DOI:10.1246/bcsj.63.3595

Reference yield: 78.0%

3-Phenyl-8a-trimethylsilanyloxy-4a,5,6,7,8,8a-hexahydro-4H-benzo[e][1,2]oxazine (109925-95-3) → 3-Phenyl-8a-hydroxy-4a.5.6.7.8.8a-hexahydro-cyclohexa-1.2.4H-oxazin (26964-95-4)

Guidance literature:

With triethylamine tris(hydrogen fluoride); In dichloromethane; for 5h; Ambient temperature;

upstream raw materials:

1-(Trimethylsilyloxy)cyclohexene

2-bromo-1-phenyl-ethanone oxime

2-chloro-1-phenyl-ethanone oxime

Downstream raw materials:

4a,5,6,7,8,8a-hexahydro-8a-methoxy-4H-1,2-benzoxazine

2-phenyl-4,5,6,7-tetrahydro-1H-indole

3-Phenyl-8a-hydroxy-4a.5.6.7.8.8a-hexahydro-cyclohexa-1.2.4H-oxazin

trans-2-(2-hydroxy-1-cyclohexyl)-1-phenyl-1-ethanone oxime

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