1-[(1R,2S)-2-(benzyloxy)-3-ethoxy-1-(ethoxycarbonyl)-3-oxopropyl]-1,2-triazadien-2-ium

Base Information

• Chemical Name: 1-[(1R,2S)-2-(benzyloxy)-3-ethoxy-1-(ethoxycarbonyl)-3-oxopropyl]-1,2-triazadien-2-ium
• CAS No.: 1192356-67-4
• Molecular Formula: C₁₅H₁₉N₃O₅
• Molecular Weight: 321.333
• Mol file: 1192356-67-4.mol

Synonyms:1-[(1R,2S)-2-(benzyloxy)-3-ethoxy-1-(ethoxycarbonyl)-3-oxopropyl]-1,2-triazadien-2-ium

Chemical Property of 1-[(1R,2S)-2-(benzyloxy)-3-ethoxy-1-(ethoxycarbonyl)-3-oxopropyl]-1,2-triazadien-2-ium

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-[(1R,2S)-2-(benzyloxy)-3-ethoxy-1-(ethoxycarbonyl)-3-oxopropyl]-1,2-triazadien-2-ium

There total 1 articles about 1-[(1R,2S)-2-(benzyloxy)-3-ethoxy-1-(ethoxycarbonyl)-3-oxopropyl]-1,2-triazadien-2-ium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1-[(1R,2S)-3-ethoxy-1-(ethoxycarbonyl)-2-hydroxy-3-oxopropyl]-1,2-triazadien-2-ium (101924-62-3) + benzyl bromide (100-39-0) → 1-[(1R,2S)-2-(benzyloxy)-3-ethoxy-1-(ethoxycarbonyl)-3-oxopropyl]-1,2-triazadien-2-ium (1192356-67-4)

Guidance literature:

With silver(l) oxide; In dichloromethane; at 20 ℃; for 10h;

DOI:10.1016/j.tetasy.2009.07.004

Reference yield:

1-[(1R,2S)-2-(benzyloxy)-3-ethoxy-1-(ethoxycarbonyl)-3-oxopropyl]-1,2-triazadien-2-ium (1192356-67-4) → C11H17NO3

Guidance literature:

1-[(1R,2S)-2-(benzyloxy)-3-ethoxy-1-(ethoxycarbonyl)-3-oxopropyl]-1,2-triazadien-2-ium; With lithium aluminium tetrahydride; In tetrahydrofuran; for 4h; Reflux;

With ammonium chloride; In tetrahydrofuran; water;

DOI:10.1016/j.tetasy.2009.07.004

upstream raw materials:

1-[(1R,2S)-3-ethoxy-1-(ethoxycarbonyl)-2-hydroxy-3-oxopropyl]-1,2-triazadien-2-ium

benzyl bromide