3,5-di-tert-butylsalicyl tosylhydrazone

Base Information

Chemical Name:3,5-di-tert-butylsalicyl tosylhydrazone
CAS No.:1429498-07-6
Molecular Formula:C₂₂H₃₀N₂O₃S
Molecular Weight:402.558
Hs Code.:

Synonyms:3,5-di-tert-butylsalicyl tosylhydrazone

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Chemical Property of 3,5-di-tert-butylsalicyl tosylhydrazone

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Technology Process of 3,5-di-tert-butylsalicyl tosylhydrazone

There total 1 articles about 3,5-di-tert-butylsalicyl tosylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 37942-07-7
3,5-di-tert-butyl-2-hydroxybenzaldehyde

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 1429498-07-6
3,5-di-tert-butylsalicyl tosylhydrazone

Guidance literature:: In methanol; at 60 ℃; for 5h;
DOI:10.1039/c4ob01979b

Reference yield: 93.0%

: 588-72-7,1340-14-3
[(E)-2-bromoethenyl]benzene

: 1429498-07-6
3,5-di-tert-butylsalicyl tosylhydrazone

: 76336-90-8
6,8-di-tert-butyl-2-phenyl-2H-chromene

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; potassium carbonate; tricyclohexylphosphine tetrafluoroborate; In 1,4-dioxane; at 100 ℃; for 12h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c4ob01979b

Reference yield: 92.0%

: 853304-33-3
3-iodo-4-phenyl-2H-benzopyran

: 1429498-07-6
3,5-di-tert-butylsalicyl tosylhydrazone

: 9,11-di-tert-butyl-12a-phenyl-6,12a-dihydrochromeno[4,3-b]-chromene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; at 110 ℃; for 10h; Inert atmosphere;
DOI:10.1021/acs.joc.5b00500