5-benzyl 1-tert-butyl hexahydro-1H-pyrrolo[3,2-c]pyridine-1,5(6H)-dicarboxylate

Base Information

Chemical Name:5-benzyl 1-tert-butyl hexahydro-1H-pyrrolo[3,2-c]pyridine-1,5(6H)-dicarboxylate
CAS No.:1312784-22-7
Molecular Formula:C₂₀H₂₈N₂O₄
Molecular Weight:360.453
Hs Code.:

Synonyms:5-benzyl 1-tert-butyl hexahydro-1H-pyrrolo[3,2-c]pyridine-1,5(6H)-dicarboxylate

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Chemical Property of 5-benzyl 1-tert-butyl hexahydro-1H-pyrrolo[3,2-c]pyridine-1,5(6H)-dicarboxylate

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Technology Process of 5-benzyl 1-tert-butyl hexahydro-1H-pyrrolo[3,2-c]pyridine-1,5(6H)-dicarboxylate

There total 1 articles about 5-benzyl 1-tert-butyl hexahydro-1H-pyrrolo[3,2-c]pyridine-1,5(6H)-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1147422-00-1,848410-13-9
tert-butyl octahydro-1H-pyrrolo[3,2-c]pyridine-1-carboxylate

: 501-53-1,94274-21-2
benzyl chloroformate

: 1312784-22-7
5-benzyl 1-tert-butyl hexahydro-1H-pyrrolo[3,2-c]pyridine-1,5(6H)-dicarboxylate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 4h;

Reference yield: 100.0%

: 1312784-22-7
5-benzyl 1-tert-butyl hexahydro-1H-pyrrolo[3,2-c]pyridine-1,5(6H)-dicarboxylate

: 1312784-23-8
benzyl hexahydro-1H-pyrrolo[3,2-c]pyridine-5(6H)-carboxylate hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 1h;

Reference yield:

: 1312784-22-7
5-benzyl 1-tert-butyl hexahydro-1H-pyrrolo[3,2-c]pyridine-1,5(6H)-dicarboxylate

: 1312784-24-9
benzyl 1-methylhexahydro-1H-pyrrolo[3,2-c]pyridine-5(6H)-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C

2.1: water; methanol / 1 h / 20 °C

2.2: 20 h / 20 °C

2.3: pH 11

With hydrogenchloride; In 1,4-dioxane; methanol; water;