7-[3-(N-3-ethynylphenylcarbamoyl)-4-methoxyphenylamino]-7-oxoheptanoic acid

Base Information

Chemical Name:7-[3-(N-3-ethynylphenylcarbamoyl)-4-methoxyphenylamino]-7-oxoheptanoic acid
CAS No.:1391013-36-7
Molecular Formula:C₂₃H₂₄N₂O₅
Molecular Weight:408.454
Hs Code.:

Synonyms:7-[3-(N-3-ethynylphenylcarbamoyl)-4-methoxyphenylamino]-7-oxoheptanoic acid

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Chemical Property of 7-[3-(N-3-ethynylphenylcarbamoyl)-4-methoxyphenylamino]-7-oxoheptanoic acid

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Technology Process of 7-[3-(N-3-ethynylphenylcarbamoyl)-4-methoxyphenylamino]-7-oxoheptanoic acid

There total 5 articles about 7-[3-(N-3-ethynylphenylcarbamoyl)-4-methoxyphenylamino]-7-oxoheptanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1304351-75-4
C₁₆H₁₄N₂O₂

: 10521-07-0
pimelic acid anhydride

: 1391013-36-7
7-[3-(N-3-ethynylphenylcarbamoyl)-4-methoxyphenylamino]-7-oxoheptanoic acid

Guidance literature:: With triethylamine; In tetrahydrofuran;
DOI:10.1016/j.bmc.2012.05.034

Reference yield:

: 1330841-08-1
N-(3-ethynylphenyl)-2-methoxy-5-nitrobenzamide

: 1391013-36-7
7-[3-(N-3-ethynylphenylcarbamoyl)-4-methoxyphenylamino]-7-oxoheptanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: iron; acetic acid / tetrahydrofuran; ethanol / 7 h / Reflux

1.2: pH 10 / Saturated solution

2.1: triethylamine / tetrahydrofuran

With iron; acetic acid; triethylamine; In tetrahydrofuran; ethanol;
DOI:10.1016/j.bmc.2012.05.034

Reference yield:

: 1352440-70-0
N-(3-ethynylphenyl)-2-hydroxy-5-nitrobenzamide

: 1391013-36-7
7-[3-(N-3-ethynylphenylcarbamoyl)-4-methoxyphenylamino]-7-oxoheptanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetone / 3 h / Reflux

2.1: iron; acetic acid / tetrahydrofuran; ethanol / 7 h / Reflux

2.2: pH 10 / Saturated solution

3.1: triethylamine / tetrahydrofuran

With iron; potassium carbonate; acetic acid; triethylamine; In tetrahydrofuran; ethanol; acetone;
DOI:10.1016/j.bmc.2012.05.034