(S)-2-[(1-tert-Butoxycarbonylamino-cyclopentanecarbonyl)-amino]-3-(4-hydroxy-phenyl)-propionic acid hexyl ester

Base Information

Chemical Name:(S)-2-[(1-tert-Butoxycarbonylamino-cyclopentanecarbonyl)-amino]-3-(4-hydroxy-phenyl)-propionic acid hexyl ester
CAS No.:1026041-62-2
Molecular Formula:C₂₆H₄₀N₂O₆
Molecular Weight:476.613
Hs Code.:

Synonyms:(S)-2-[(1-tert-Butoxycarbonylamino-cyclopentanecarbonyl)-amino]-3-(4-hydroxy-phenyl)-propionic acid hexyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-[(1-tert-Butoxycarbonylamino-cyclopentanecarbonyl)-amino]-3-(4-hydroxy-phenyl)-propionic acid hexyl ester

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Technology Process of (S)-2-[(1-tert-Butoxycarbonylamino-cyclopentanecarbonyl)-amino]-3-(4-hydroxy-phenyl)-propionic acid hexyl ester

There total 1 articles about (S)-2-[(1-tert-Butoxycarbonylamino-cyclopentanecarbonyl)-amino]-3-(4-hydroxy-phenyl)-propionic acid hexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 35264-09-6
1-(tert-butoxycarbonylamino)cyclopentanecarboxylic acid

: 94326-61-1
hexyl L-tyrosinate

: 1026041-62-2
(S)-2-[(1-tert-Butoxycarbonylamino-cyclopentanecarbonyl)-amino]-3-(4-hydroxy-phenyl)-propionic acid hexyl ester

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1021/jm960323z

Reference yield:

: 1026041-62-2
(S)-2-[(1-tert-Butoxycarbonylamino-cyclopentanecarbonyl)-amino]-3-(4-hydroxy-phenyl)-propionic acid hexyl ester

: (S)-2-[(1-Amino-cyclopentanecarbonyl)-amino]-3-(4-hydroxy-phenyl)-propionic acid hexyl ester; hydrochloride

Guidance literature:: With hydrogenchloride; In dichloromethane; for 0.25h;
DOI:10.1021/jm960323z

Reference yield:

: 1026041-62-2
(S)-2-[(1-tert-Butoxycarbonylamino-cyclopentanecarbonyl)-amino]-3-(4-hydroxy-phenyl)-propionic acid hexyl ester

: (S)-2-{[1-((S)-2-Acetylsulfanyl-3-methyl-butyrylamino)-cyclopentanecarbonyl]-amino}-3-(4-hydroxy-phenyl)-propionic acid hexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: HCl / CH₂Cl₂ / 0.25 h

2: Et₃N, 1,3-dicyclohexylcarbodiimide, 1-hydroxy-7-azabenzotriazole / CH₂Cl₂ / 16 h

With hydrogenchloride; 1-hydroxy-7-aza-benzotriazole; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1021/jm960323z