C₄₅H₄₅NO₅S₄

Base Information

Chemical Name:C₄₅H₄₅NO₅S₄
CAS No.:1383942-49-1
Molecular Formula:C₄₅H₄₅NO₅S₄
Molecular Weight:808.12
Hs Code.:

C<sub>45</sub>H<sub>45</sub>NO<sub>5</sub>S<sub>4</sub>

Synonyms:C₄₅H₄₅NO₅S₄

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Chemical Property of C₄₅H₄₅NO₅S₄

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Technology Process of C₄₅H₄₅NO₅S₄

There total 2 articles about C₄₅H₄₅NO₅S₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 175922-79-9
tributyl(2,3-dihydrothieno[3,4-b][1,4]dioxin-5-yl)-stannane

: 1383942-49-1
C₄₅H₄₅NO₅S₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / para-xylene / 5 h / Inert atmosphere; Reflux

2.1: trichlorophosphate / 1 h / 0 °C

2.2: 1 h / 0 - 20 °C

2.3: pH 10

3.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 20 °C

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / para-xylene / 24 h / Inert atmosphere; Reflux

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; trichlorophosphate; In para-xylene; N,N-dimethyl-formamide; 1.1: Stille coupling / 2.2: Vilsmeier-Haack reaction / 4.1: Stille coupling;
DOI:10.1016/j.tet.2012.04.113

Reference yield:

: 1383942-36-6
C₁₄H₈O₂S₄

: 1383942-49-1
C₄₅H₄₅NO₅S₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: trichlorophosphate / 1 h / 0 °C

1.2: 1 h / 0 - 20 °C

1.3: pH 10

2.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 20 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / para-xylene / 24 h / Inert atmosphere; Reflux

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; trichlorophosphate; In para-xylene; N,N-dimethyl-formamide; 1.2: Vilsmeier-Haack reaction / 3.1: Stille coupling;
DOI:10.1016/j.tet.2012.04.113