3-(4-methylbenzoyl)-1-(4-nitrophenoxycarbonyl)-7-pyridin-4-ylindolizine

Base Information

Chemical Name:3-(4-methylbenzoyl)-1-(4-nitrophenoxycarbonyl)-7-pyridin-4-ylindolizine
CAS No.:853268-94-7
Molecular Formula:C₂₈H₁₉N₃O₅
Molecular Weight:477.476
Hs Code.:

Synonyms:3-(4-methylbenzoyl)-1-(4-nitrophenoxycarbonyl)-7-pyridin-4-ylindolizine

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Chemical Property of 3-(4-methylbenzoyl)-1-(4-nitrophenoxycarbonyl)-7-pyridin-4-ylindolizine

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Technology Process of 3-(4-methylbenzoyl)-1-(4-nitrophenoxycarbonyl)-7-pyridin-4-ylindolizine

There total 3 articles about 3-(4-methylbenzoyl)-1-(4-nitrophenoxycarbonyl)-7-pyridin-4-ylindolizine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 35665-87-3
propynoic acid-4-nitrophenylester

: 1-(4-methylbenzoylmethyl)-[4,4']bipyridinium bromide

: 853268-94-7
3-(4-methylbenzoyl)-1-(4-nitrophenoxycarbonyl)-7-pyridin-4-ylindolizine

Guidance literature:: With 1-methyl-pyrrolidin-2-one; triethylamine; at 0 ℃; for 48h;
DOI:10.1016/j.tet.2005.02.063

Reference yield:

: 553-26-4
4,4'-bipyridine

: 853268-94-7
3-(4-methylbenzoyl)-1-(4-nitrophenoxycarbonyl)-7-pyridin-4-ylindolizine

Guidance literature:: Multi-step reaction with 2 steps

1: acetone / 10 h / 40 °C

2: 53 percent / triethylamine; N-methylpyrrolidone / 48 h / 0 °C

With 1-methyl-pyrrolidin-2-one; triethylamine; In acetone;
DOI:10.1016/j.tet.2005.02.063

Reference yield:

: 619-41-0
4-(bromoacetyl)toluene

: 853268-94-7
3-(4-methylbenzoyl)-1-(4-nitrophenoxycarbonyl)-7-pyridin-4-ylindolizine

Guidance literature:: Multi-step reaction with 2 steps

1: acetone / 10 h / 40 °C

2: 53 percent / triethylamine; N-methylpyrrolidone / 48 h / 0 °C

With 1-methyl-pyrrolidin-2-one; triethylamine; In acetone;
DOI:10.1016/j.tet.2005.02.063