6-{[4-(dimethylamino)phenyl](1-piperidinyl)methyl}-1,3-benzodioxol-5-ol

Base Information

Chemical Name:6-{[4-(dimethylamino)phenyl](1-piperidinyl)methyl}-1,3-benzodioxol-5-ol
CAS No.:102616-83-1
Molecular Formula:C₂₁H₂₆N₂O₃
Molecular Weight:354.449
Hs Code.:

Synonyms:6-{[4-(dimethylamino)phenyl](1-piperidinyl)methyl}-1,3-benzodioxol-5-ol

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Chemical Property of 6-{[4-(dimethylamino)phenyl](1-piperidinyl)methyl}-1,3-benzodioxol-5-ol

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Technology Process of 6-{[4-(dimethylamino)phenyl](1-piperidinyl)methyl}-1,3-benzodioxol-5-ol

There total 1 articles about 6-{[4-(dimethylamino)phenyl](1-piperidinyl)methyl}-1,3-benzodioxol-5-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 110-89-4
piperidine

: 533-31-3
Sesamol

: 100-10-7
4-dimethylamino-benzaldehyde

: 102616-83-1
6-{[4-(dimethylamino)phenyl](1-piperidinyl)methyl}-1,3-benzodioxol-5-ol

Guidance literature:: In methanol; Heating;
DOI:10.1002/jhet.5570220412

Reference yield: 85.0%

: 3262-89-3
triphenylboroxine

: 102616-83-1
6-{[4-(dimethylamino)phenyl](1-piperidinyl)methyl}-1,3-benzodioxol-5-ol

: C₂₂H₂₁NO₃

Guidance literature:: With [RhCl((R,R)-ferrocenyl-tfb*)]₂; potassium hydroxide; In 1,4-dioxane; at 20 - 40 ℃; for 15h; enantioselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1021/jacs.5b03277

Reference yield: 63.0%

: 19261-37-1
2-chloro-3-phenyl-propionaldehyde

: 102616-83-1
6-{[4-(dimethylamino)phenyl](1-piperidinyl)methyl}-1,3-benzodioxol-5-ol

: (7S,8S)-7-benzyl-8-(4-(dimethylamino)phenyl)-7,8-dihydro-6H-[1,3]dioxolo[4,5-g]chromen-6-one

Guidance literature:: With C₂₂H₂₄N₃⁽¹⁺⁾*BF₄^(1-); sodium acetate; In dichloromethane; at 40 ℃; for 24h; stereoselective reaction; Schlenk technique; Sealed tube; Inert atmosphere;
DOI:10.1021/acs.orglett.7b02883