para-iodobenzenesulfonyl azide

Base Information

• Chemical Name: para-iodobenzenesulfonyl azide
• CAS No.: 50875-89-3
• Molecular Formula: C₆H₄IN₃O₂S
• Molecular Weight: 309.087
• Mol file: 50875-89-3.mol

Synonyms:para-iodobenzenesulfonyl azide

Chemical Property of para-iodobenzenesulfonyl azide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of para-iodobenzenesulfonyl azide

There total 1 articles about para-iodobenzenesulfonyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

p-Iodobenzenesulfonyl chloride (98-61-3) → para-iodobenzenesulfonyl azide (50875-89-3)

Guidance literature:

With sodium azide; In water; acetone; at 0 ℃; for 2h;

DOI:10.1039/d0cc01647k

Reference yield: 94.0%

para-iodobenzenesulfonyl azide (50875-89-3) + benzoic acid (65-85-0,8013-63-6) → N-((4-iodophenyl)sulfonyl)benzamide

Guidance literature:

With dicobalt octacarbonyl; tert-butylisonitrile; In acetonitrile; at 80 ℃; for 4h;

DOI:10.1021/acs.joc.8b01300

Reference yield: 88.0%

1-methyl-2-carboxy-1,2-dicarba-closo-dodecaborane(12) (14078-85-4) + para-iodobenzenesulfonyl azide (50875-89-3) → C9H18B10INO2S

Guidance literature:

With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; sodium acetate; silver(I) triflimide; In 1,2-dichloro-ethane; at 85 ℃; for 10h; regioselective reaction; Inert atmosphere; Schlenk technique;

DOI:10.1002/ejoc.201601537

upstream raw materials:

p-Iodobenzenesulfonyl chloride

Downstream raw materials:

C₁₄H₁₆INO₃S

C₁₄H₁₆IN₃O₃S