C₃₄H₃₄N₈O₇S

Base Information

Chemical Name:C₃₄H₃₄N₈O₇S
CAS No.:848761-15-9
Molecular Formula:C₃₄H₃₄N₈O₇S
Molecular Weight:698.759
Hs Code.:

C<sub>34</sub>H<sub>34</sub>N<sub>8</sub>O<sub>7</sub>S

Synonyms:C₃₄H₃₄N₈O₇S

Suppliers and Price of C₃₄H₃₄N₈O₇S

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₄H₃₄N₈O₇S

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₄H₃₄N₈O₇S

There total 15 articles about C₃₄H₃₄N₈O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 848761-14-8
C₃₄H₃₆N₈O₈S

: 848761-15-9
C₃₄H₃₄N₈O₇S

Guidance literature:: With diethylamino-sulfur trifluoride; In dichloromethane; at -78 ℃; for 2h;
DOI:10.1039/b416530f

Reference yield:

: 848761-02-4
2-((S)-2-benzyloxy-1-{[2-(tert-butoxycarbonylaminomethyl)oxazole-4-carbonyl]amino}ethyl)oxazole-4-carboxylic acid methyl ester

: 848761-15-9
C₃₄H₃₄N₈O₇S

Guidance literature:: Multi-step reaction with 11 steps

1.1: 81 percent / H₂ / Pd(OH)2/C / methanol; tetrahydrofuran / 20 °C

2.1: (diethylamino)sulfur trifluoride / CH₂Cl₂ / 1.5 h / -78 °C

2.2: 57 percent / BrCCl₃; DBU / CH₂Cl₂ / 24 h / 0 - 20 °C

3.1: 88 percent / aq. NaOH / tetrahydrofuran / 24 h / 20 °C

4.1: 87 percent / 1-(3-(dimethylamino)propyl)-3-ethylcarbodiimide*HCl; 1-hydroxybenzotriazole; 4-methylmorpholine / CH₂Cl₂ / 24 h / 0 - 20 °C

5.1: 50 percent / Lawesson's reagent / tetrahydrofuran / 18 h / Heating

6.1: 91 percent / HCl / dioxane / 24 h / 20 °C

7.1: 82 percent / 1-(3-(dimethylamino)propyl)-3-ethylcarbodiimide*HCl; 1-hydroxybenzotriazole; 4-methylmorpholine / CH₂Cl₂ / 48 h / 0 - 20 °C

8.1: aq. NaOH / tetrahydrofuran / 24 h / 20 °C

9.1: HCl / dioxane / 18 h / 20 °C

10.1: 75 percent / O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium*PF₆; 4-methylmorpholine / CH₂Cl₂; dimethylformamide / 72 h / 0 - 20 °C

11.1: 89 percent / (diethylamino)sulfur trifluoride / CH₂Cl₂ / 2 h / -78 °C

With Lawessons reagent; 4-methyl-morpholine; hydrogenchloride; sodium hydroxide; diethylamino-sulfur trifluoride; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; HATU; palladium dihydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b416530f

Reference yield:

: 848761-00-2
(S)-2-benzyloxy-1-(4-methoxycarbonyloxazol-2-yl)ethylammonium chloride

: 848761-15-9
C₃₄H₃₄N₈O₇S

Guidance literature:: Multi-step reaction with 12 steps

1.1: 56 percent / 1-(3-(dimethylamino)propyl)-3-ethylcarbodiimide*HCl; 1-hydroxybenzotriazole; 4-methylmorpholine / CH₂Cl₂ / 24 h / 0 - 20 °C

2.1: 81 percent / H₂ / Pd(OH)2/C / methanol; tetrahydrofuran / 20 °C

3.1: (diethylamino)sulfur trifluoride / CH₂Cl₂ / 1.5 h / -78 °C

3.2: 57 percent / BrCCl₃; DBU / CH₂Cl₂ / 24 h / 0 - 20 °C

4.1: 88 percent / aq. NaOH / tetrahydrofuran / 24 h / 20 °C

5.1: 87 percent / 1-(3-(dimethylamino)propyl)-3-ethylcarbodiimide*HCl; 1-hydroxybenzotriazole; 4-methylmorpholine / CH₂Cl₂ / 24 h / 0 - 20 °C

6.1: 50 percent / Lawesson's reagent / tetrahydrofuran / 18 h / Heating

7.1: 91 percent / HCl / dioxane / 24 h / 20 °C

8.1: 82 percent / 1-(3-(dimethylamino)propyl)-3-ethylcarbodiimide*HCl; 1-hydroxybenzotriazole; 4-methylmorpholine / CH₂Cl₂ / 48 h / 0 - 20 °C

9.1: aq. NaOH / tetrahydrofuran / 24 h / 20 °C

10.1: HCl / dioxane / 18 h / 20 °C

11.1: 75 percent / O-(7-azabenzotriazol-1-yl)-N,N,N',N'-tetramethyluronium*PF₆; 4-methylmorpholine / CH₂Cl₂; dimethylformamide / 72 h / 0 - 20 °C

12.1: 89 percent / (diethylamino)sulfur trifluoride / CH₂Cl₂ / 2 h / -78 °C

With Lawessons reagent; 4-methyl-morpholine; hydrogenchloride; sodium hydroxide; diethylamino-sulfur trifluoride; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; HATU; palladium dihydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b416530f