N,N-bis(4-nitrophenyl)-N',N'-bis[4-(2-phenyl-2-isopropyl)phenyl]-1,4-phenylenediamine

Base Information

Chemical Name:N,N-bis(4-nitrophenyl)-N',N'-bis[4-(2-phenyl-2-isopropyl)phenyl]-1,4-phenylenediamine
CAS No.:1246049-04-6
Molecular Formula:C₄₈H₄₂N₄O₄
Molecular Weight:738.886
Hs Code.:

Synonyms:N,N-bis(4-nitrophenyl)-N',N'-bis[4-(2-phenyl-2-isopropyl)phenyl]-1,4-phenylenediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-bis(4-nitrophenyl)-N',N'-bis[4-(2-phenyl-2-isopropyl)phenyl]-1,4-phenylenediamine

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Technology Process of N,N-bis(4-nitrophenyl)-N',N'-bis[4-(2-phenyl-2-isopropyl)phenyl]-1,4-phenylenediamine

There total 4 articles about N,N-bis(4-nitrophenyl)-N',N'-bis[4-(2-phenyl-2-isopropyl)phenyl]-1,4-phenylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1243278-14-9
bis[4-(2-phenyl-2-isopropyl)phenyl]-4-aminophenylamine

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 1246049-04-6
N,N-bis(4-nitrophenyl)-N',N'-bis[4-(2-phenyl-2-isopropyl)phenyl]-1,4-phenylenediamine

Guidance literature:: With cesium fluoride; In dimethyl sulfoxide; at 120 ℃; for 24h;
DOI:10.1016/j.polymer.2010.07.023

Reference yield:

: 1243278-12-7
bis[4-(2-phenyl-2-isopropyl)phenyl]-4-nitrophenylamine

: 1246049-04-6
N,N-bis(4-nitrophenyl)-N',N'-bis[4-(2-phenyl-2-isopropyl)phenyl]-1,4-phenylenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / palladium 10% on activated carbon / ethanol / 90 °C

2: cesium fluoride / dimethyl sulfoxide / 24 h / 120 °C

With hydrazine hydrate; cesium fluoride; palladium 10% on activated carbon; In ethanol; dimethyl sulfoxide;

Reference yield:

: 10081-67-1
bis[4-(2-phenyl-2-propyl)phenyl]amine

: 1246049-04-6
N,N-bis(4-nitrophenyl)-N',N'-bis[4-(2-phenyl-2-isopropyl)phenyl]-1,4-phenylenediamine

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / dimethyl sulfoxide / 48 h / 120 °C

2: hydrazine hydrate / palladium 10% on activated carbon / ethanol / 90 °C

3: cesium fluoride / dimethyl sulfoxide / 24 h / 120 °C

With sodium hydride; hydrazine hydrate; cesium fluoride; palladium 10% on activated carbon; In ethanol; dimethyl sulfoxide;