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Antioxidant 445
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Bis[4-(2-phenyl-2-propyl)phenyl]amine Manufacturer/High quality/Best price/In stock
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High quality 4,4’-Bis(Α,Α’-Dimethylbenzyl) Diphenylamine supplier in China
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High purity 10081-67-1
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USD $ 100.0-500.0 / Gram 1 Gram 99999 Gram/Year Hangzhou Dingyan Chem Co., Ltd Contact Supplier
4,4'-Bis-(α,α'-dimethylbenzyl)-diphenylamine
Cas No: 10081-67-1
No Data No Data No Data Chemwill Asia Co., Ltd. Contact Supplier
Factory Supply 4-(1-methyl-1-phenylethyl)-N-[4-(1-methyl-1-phenylethyl)phenyl]aniline
Cas No: 10081-67-1
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6-(1-cyclohex-2-enyl)-1,3,5-triazine-2,4-diamine
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Bis[4-(2-phenyl-2-propyl)phenyl]amine
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10081-67-1
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10081-67-1 Usage

InChI:InChI=1/C30H31N/c1-29(2,23-11-7-5-8-12-23)25-15-19-27(20-16-25)31-28-21-17-26(18-22-28)30(3,4)24-13-9-6-10-14-24/h5-22,31H,1-4H3

10081-67-1SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 10, 2017

Revision Date: Aug 10, 2017

1.Identification

1.1 GHS Product identifier

Product name Naugard 445

1.2 Other means of identification

Product number -
Other names 4-(2-phenylpropan-2-yl)-N-[4-(2-phenylpropan-2-yl)phenyl]aniline

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:10081-67-1 SDS

10081-67-1Synthetic route

diphenylamine
122-39-4

diphenylamine

isopropenylbenzene
98-83-9

isopropenylbenzene

A

bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

B

4-(α,α-dimethylbenzyl)diphenylamine

4-(α,α-dimethylbenzyl)diphenylamine

Conditions
ConditionsYield
With Al-MSU-G at 90℃; for 6h; Product distribution; Further Variations:; Reagents; Temperatures; reaction time;A 97.2%
B n/a
With acid-treated clay catalyst Engelhard F-24 In o-xylene at 89.9℃; for 12h; Product distribution; Irradiation; other alkylating agent, var. catalyst, var. temp, var. solvent, var. time, also without sonication, and in air, also reused catalysts;
diphenylamine
122-39-4

diphenylamine

isopropenylbenzene
98-83-9

isopropenylbenzene

bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

Conditions
ConditionsYield
With zinc(II) chloride In ethanol; 1,2-dichloro-ethane at 185℃; Solvent; Temperature; Reagent/catalyst; Flow reactor; regioselective reaction;89%
Stage #1: diphenylamine With tin(ll) chloride; magnesium chloride Heating;
Stage #2: isopropenylbenzene at 130 - 140℃; for 1.5h; Reagent/catalyst; Temperature;
85%
With 2-methylbenzene-1,4-diol In toluene at 60 - 125℃; Inert atmosphere;38.5 g
N-phenyl-1-naphthylamine
90-30-2

N-phenyl-1-naphthylamine

diphenylamine
122-39-4

diphenylamine

isopropenylbenzene
98-83-9

isopropenylbenzene

A

4-nonyldiphenylamine

4-nonyldiphenylamine

B

4-α-methylstyryl-4'-nonyldiphenylamine

4-α-methylstyryl-4'-nonyldiphenylamine

C

4,4'-dinonyldiphenylamine

4,4'-dinonyldiphenylamine

D

bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

E

4-(α,α-dimethylbenzyl)diphenylamine

4-(α,α-dimethylbenzyl)diphenylamine

Conditions
ConditionsYield
Stage #1: N-phenyl-1-naphthylamine; diphenylamine; Fulcat 22B at 220℃; under 15.0015 Torr; for 1h;
Stage #2: 2,4-dimethyl-1-heptene at 130 - 220℃; for 6.5h;
Stage #3: isopropenylbenzene at 130 - 134℃; for 3h; Product distribution / selectivity;
diphenylamine
122-39-4

diphenylamine

isopropenylbenzene
98-83-9

isopropenylbenzene

A

4-nonyldiphenylamine

4-nonyldiphenylamine

B

4-α-methylstyryl-4'-nonyldiphenylamine

4-α-methylstyryl-4'-nonyldiphenylamine

C

4,4'-dinonyldiphenylamine

4,4'-dinonyldiphenylamine

D

bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

E

4-(α,α-dimethylbenzyl)diphenylamine

4-(α,α-dimethylbenzyl)diphenylamine

Conditions
ConditionsYield
Stage #1: 2,4-dimethyl-1-heptene; diphenylamine; Fulcat 22B at 80 - 220℃; under 15.0015 Torr; for 5.5 - 7.5h;
Stage #2: isopropenylbenzene at 130 - 134℃; for 3h; Product distribution / selectivity;
bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

ethyl 10-bromoanthracene-9-carboxylate

ethyl 10-bromoanthracene-9-carboxylate

ethyl 10-[bis[4-(1-methyl-1-phenylethyl)phenyl]amino]anthracene-9-carboxylate

ethyl 10-[bis[4-(1-methyl-1-phenylethyl)phenyl]amino]anthracene-9-carboxylate

Conditions
ConditionsYield
With tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate In toluene at 90℃; for 3h; Inert atmosphere;90%
9,10-Dibromoanthracene
523-27-3

9,10-Dibromoanthracene

bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

N9,N9,N10,N10-tetrakis(4-(2-phenylpropan-2-yl)phenyl)anthracene-9,10-diamine

N9,N9,N10,N10-tetrakis(4-(2-phenylpropan-2-yl)phenyl)anthracene-9,10-diamine

Conditions
ConditionsYield
With tri-tert-butyl phosphine; palladium diacetate; potassium carbonate In toluene for 10h; Reflux;80%
ethyl 2-bromoisobutyrate
600-00-0

ethyl 2-bromoisobutyrate

bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

3,3-dimethyl-5-(2-phenylpropan-2-yl)-1-(4-(2-phenylpropan-2-yl)phenyl)indolin-2-one

3,3-dimethyl-5-(2-phenylpropan-2-yl)-1-(4-(2-phenylpropan-2-yl)phenyl)indolin-2-one

Conditions
ConditionsYield
With [2,2]bipyridinyl; copper diacetate; potassium carbonate In acetonitrile at 120℃; for 12h; Schlenk technique; Inert atmosphere;80%
2-bromospiro[fluorenyl-9,8'-indolo[3,2,1-de]acridine]

2-bromospiro[fluorenyl-9,8'-indolo[3,2,1-de]acridine]

bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

C61H48N2

C61H48N2

Conditions
ConditionsYield
With bis(tri-t-butylphosphine)palladium(0); sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene for 3h; Inert atmosphere; Heating;70%
1-bromo-2,3-dichlorobenzene
56961-77-4

1-bromo-2,3-dichlorobenzene

bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

C66H63ClN2

C66H63ClN2

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate at 130℃; Inert atmosphere;66.2%
bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

4-Fluoronitrobenzene
350-46-9

4-Fluoronitrobenzene

bis[4-(2-phenyl-2-isopropyl)phenyl]-4-nitrophenylamine
1243278-12-7

bis[4-(2-phenyl-2-isopropyl)phenyl]-4-nitrophenylamine

Conditions
ConditionsYield
With sodium hydride In dimethyl sulfoxide at 120℃; for 24h;63%
With sodium hydride In dimethyl sulfoxide at 120℃; for 48h;50%
With sodium hydride In dimethyl sulfoxide at 120℃; for 48h;50%
1.4-dibromobenzene
106-37-6

1.4-dibromobenzene

bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

N-(4-bromophenyl)-4-(2-phenylpropan-2-yl)-N-(4-(2-phenylpropan-2-yl)phenyl)benzeneamine
1310961-36-4

N-(4-bromophenyl)-4-(2-phenylpropan-2-yl)-N-(4-(2-phenylpropan-2-yl)phenyl)benzeneamine

Conditions
ConditionsYield
With 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; sodium t-butanolate In toluene at 120℃; for 7h; Inert atmosphere;62%
iodobenzene
591-50-4

iodobenzene

bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

C36H35N
259218-10-5

C36H35N

Conditions
ConditionsYield
With 1,1'-bis-(diphenylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate In toluene for 8h; Buchwald-Hartwig reaction; Reflux; Inert atmosphere;55%
With 1,1'-bis-(diphenylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate In toluene for 8h; Inert atmosphere; Reflux;55%
4,4,4-trifluorobutyric acid
406-93-9

4,4,4-trifluorobutyric acid

bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

4-(2-phenylpropan-2-yl)-N-(4-(2-phenylpropan-2-yl)phenyl)-N-(3,3,3-trifluoropropyl)aniline

4-(2-phenylpropan-2-yl)-N-(4-(2-phenylpropan-2-yl)phenyl)-N-(3,3,3-trifluoropropyl)aniline

Conditions
ConditionsYield
With di-tert-butyl peroxide; copper(II) hexafluoroacetylacetonate; 9-mesitylacridine at 35℃; for 24h; Inert atmosphere; Irradiation;51%
bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

7-bromo-10-hexyl-10H-phenothiazine-3-carbaldehyde
312924-97-3

7-bromo-10-hexyl-10H-phenothiazine-3-carbaldehyde

7-(bis(4-(2-phenylpropan-2-yl)phenyl)amino)-10-hexyl-10H-phenothiazine-3-carbaldehyde
1618093-71-2

7-(bis(4-(2-phenylpropan-2-yl)phenyl)amino)-10-hexyl-10H-phenothiazine-3-carbaldehyde

Conditions
ConditionsYield
With tri-tert-butyl phosphine; potassium tert-butylate; palladium diacetate In toluene Reflux; Inert atmosphere;45%
carbon tetrabromide
558-13-4

carbon tetrabromide

bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

2,7-bis(1-methyl-1-phenylethyl)-N,N-bis[4-(1-methyl-1-phenylethyl)phenyl]acridin-9-amine

2,7-bis(1-methyl-1-phenylethyl)-N,N-bis[4-(1-methyl-1-phenylethyl)phenyl]acridin-9-amine

Conditions
ConditionsYield
In toluene at 20℃; Rate constant; Irradiation; photoinduced reaction of diarylamines with CBr4; spectral study; intermediates formation; spectral and kinetic properties of intermediates;
In toluene at 20℃; Irradiation;
In hexane Irradiation;
bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: sodium hydride / dimethyl sulfoxide / 48 h / 120 °C
2: palladium on activated charcoal; hydrazine hydrate / 12 h / Reflux; Inert atmosphere
3: 1,1'-bis-(diphenylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate / toluene / 10 h / Reflux; Inert atmosphere
View Scheme
bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

bis[4-(2-phenyl-2-isopropyl)phenyl]-4-aminophenylamine
1243278-14-9

bis[4-(2-phenyl-2-isopropyl)phenyl]-4-aminophenylamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium hydride / dimethyl sulfoxide / 48 h / 120 °C
2: palladium on activated charcoal; hydrazine hydrate / 12 h / Reflux; Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1: sodium hydride / dimethyl sulfoxide / 48 h / 120 °C
2: hydrazine hydrate / palladium 10% on activated carbon / ethanol / 90 °C
View Scheme
Multi-step reaction with 2 steps
1: sodium hydride / dimethyl sulfoxide / 24 h / 120 °C
2: palladium on activated charcoal; hydrazine hydrate / ethanol / 12 h / Reflux
View Scheme
bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

N,N-bis(4-nitrophenyl)-N',N'-bis[4-(2-phenyl-2-isopropyl)phenyl]-1,4-phenylenediamine
1246049-04-6

N,N-bis(4-nitrophenyl)-N',N'-bis[4-(2-phenyl-2-isopropyl)phenyl]-1,4-phenylenediamine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: sodium hydride / dimethyl sulfoxide / 48 h / 120 °C
2: hydrazine hydrate / palladium 10% on activated carbon / ethanol / 90 °C
3: cesium fluoride / dimethyl sulfoxide / 24 h / 120 °C
View Scheme
Multi-step reaction with 3 steps
1: sodium hydride / dimethyl sulfoxide / 24 h / 120 °C
2: palladium on activated charcoal; hydrazine hydrate / ethanol / 12 h / Reflux
3: cesium fluoride / dimethyl sulfoxide / 24 h / 120 °C
View Scheme
bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

N,N-bis(4-aminophenyl)-N',N'-bis[4-(2-phenyl-2-isopropyl)phenyl]-1,4-phenylenediamine
1246048-80-5

N,N-bis(4-aminophenyl)-N',N'-bis[4-(2-phenyl-2-isopropyl)phenyl]-1,4-phenylenediamine

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: sodium hydride / dimethyl sulfoxide / 48 h / 120 °C
2: hydrazine hydrate / palladium 10% on activated carbon / ethanol / 90 °C
3: cesium fluoride / dimethyl sulfoxide / 24 h / 120 °C
4: hydrazine / palladium 10% on activated carbon / ethanol / 90 °C
View Scheme
Multi-step reaction with 4 steps
1: sodium hydride / dimethyl sulfoxide / 24 h / 120 °C
2: palladium on activated charcoal; hydrazine hydrate / ethanol / 12 h / Reflux
3: cesium fluoride / dimethyl sulfoxide / 24 h / 120 °C
4: palladium on activated charcoal; hydrazine hydrate / ethanol / 12.5 h / 90 °C / Reflux
View Scheme
1.4-dibromobenzene
106-37-6

1.4-dibromobenzene

bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

C80H79N3

C80H79N3

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; sodium t-butanolate / toluene / 7 h / 120 °C / Inert atmosphere
2: 1,1'-bis-(diphenylphosphino)ferrocene; tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate / toluene / 5 h / 110 °C / Inert atmosphere
View Scheme
bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

C39H33N3O2S
1350319-91-3

C39H33N3O2S

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium t-butanolate; tri-tert-butyl phosphine; palladium diacetate / toluene; icosane / 2 h
2: acetonitrile / 4 h / 20 °C
View Scheme
bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

C45H43N3O4S
1350319-92-4

C45H43N3O4S

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: sodium t-butanolate; tri-tert-butyl phosphine; palladium diacetate / toluene; icosane / 2 h
2: acetonitrile / 4 h / 20 °C
3: potassium carbonate / acetonitrile / 2 h / 80 °C
View Scheme
bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

C41H35N3O4S
1350319-94-6

C41H35N3O4S

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: sodium t-butanolate; tri-tert-butyl phosphine; palladium diacetate / toluene; icosane / 2 h
2: acetonitrile / 4 h / 20 °C
3: potassium carbonate / acetonitrile / 2 h / 80 °C
4: toluene-4-sulfonic acid / toluene / 4 h / 80 °C
View Scheme
2-bromothiophene
1003-09-4

2-bromothiophene

bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

C34H33NS
1350319-90-2

C34H33NS

Conditions
ConditionsYield
With tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate In icosane; toluene for 2h;43.3 g
bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

7-bromo-10-hexyl-10H-phenothiazine-3-carbaldehyde
312924-97-3

7-bromo-10-hexyl-10H-phenothiazine-3-carbaldehyde

3-(7-(bis(4-(2-phenylpropan-2-yl)phenyl)amino)-10-hexyl-10H-phenothiazin-3-yl)-2-cyanoacrylic acid
1618093-69-8

3-(7-(bis(4-(2-phenylpropan-2-yl)phenyl)amino)-10-hexyl-10H-phenothiazin-3-yl)-2-cyanoacrylic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: palladium diacetate; tri-tert-butyl phosphine; potassium tert-butylate / toluene / Reflux; Inert atmosphere
2: piperidine / acetonitrile; chloroform / 10 h / Reflux
View Scheme
(S)-epichlorohydrin
67843-74-7

(S)-epichlorohydrin

bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

C33H36ClNO

C33H36ClNO

Conditions
ConditionsYield
With acetic acid at 60 - 65℃; for 48h;
bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

(R)-3-(4,4'-bis(α,α-dimethylbenzyl))diphenylaminopropene oxide

(R)-3-(4,4'-bis(α,α-dimethylbenzyl))diphenylaminopropene oxide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: acetic acid / 48 h / 60 - 65 °C
2: sodium hydroxide / diethyl ether / 2 h / Reflux
View Scheme
bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

(S)-3-(4,4'-bis(α,α-dimethylbenzyl))diphenylaminopropene oxide

(S)-3-(4,4'-bis(α,α-dimethylbenzyl))diphenylaminopropene oxide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: acetic acid / 48 h / 60 - 65 °C
2: sodium hydroxide / diethyl ether / 2 h / Reflux
View Scheme
(R)-(-)-epichlorohydrin
51594-55-9

(R)-(-)-epichlorohydrin

bis[4-(2-phenyl-2-propyl)phenyl]amine
10081-67-1

bis[4-(2-phenyl-2-propyl)phenyl]amine

C33H36ClNO

C33H36ClNO

Conditions
ConditionsYield
With acetic acid at 60 - 65℃; for 48h;

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