(E)-3-[5-tert-Butyl-3-((E)-2-ethoxycarbonyl-vinyl)-2-methoxy-phenyl]-acrylic acid 4-nitro-phenyl ester

Base Information

Chemical Name:(E)-3-[5-tert-Butyl-3-((E)-2-ethoxycarbonyl-vinyl)-2-methoxy-phenyl]-acrylic acid 4-nitro-phenyl ester
CAS No.:73213-42-0
Molecular Formula:C₂₅H₂₇NO₇
Molecular Weight:453.492
Hs Code.:

Synonyms:(E)-3-[5-tert-Butyl-3-((E)-2-ethoxycarbonyl-vinyl)-2-methoxy-phenyl]-acrylic acid 4-nitro-phenyl ester

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Chemical Property of (E)-3-[5-tert-Butyl-3-((E)-2-ethoxycarbonyl-vinyl)-2-methoxy-phenyl]-acrylic acid 4-nitro-phenyl ester

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Technology Process of (E)-3-[5-tert-Butyl-3-((E)-2-ethoxycarbonyl-vinyl)-2-methoxy-phenyl]-acrylic acid 4-nitro-phenyl ester

There total 4 articles about (E)-3-[5-tert-Butyl-3-((E)-2-ethoxycarbonyl-vinyl)-2-methoxy-phenyl]-acrylic acid 4-nitro-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 210417-68-8
2-methoxy-5-tert-butyl-1,3-benzenedicarboxaldehyde

: 73213-42-0
(E)-3-[5-tert-Butyl-3-((E)-2-ethoxycarbonyl-vinyl)-2-methoxy-phenyl]-acrylic acid 4-nitro-phenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: CH₂Cl₂ / 12 h / Ambient temperature

2: NaOH (1 equiv)

3: phosphorus trichloride

4: pyridine

With pyridine; sodium hydroxide; phosphorus trichloride; In dichloromethane;
DOI:10.1021/ja00522a054

Reference yield:

: (E)-3-[5-tert-Butyl-3-((E)-2-ethoxycarbonyl-vinyl)-2-methoxy-phenyl]-acrylic acid

: 73213-42-0
(E)-3-[5-tert-Butyl-3-((E)-2-ethoxycarbonyl-vinyl)-2-methoxy-phenyl]-acrylic acid 4-nitro-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus trichloride

2: pyridine

With pyridine; phosphorus trichloride;
DOI:10.1021/ja00522a054

Reference yield:

: (E)-3-[5-tert-Butyl-3-((E)-2-ethoxycarbonyl-vinyl)-2-methoxy-phenyl]-acrylic acid ethyl ester

: 73213-42-0
(E)-3-[5-tert-Butyl-3-((E)-2-ethoxycarbonyl-vinyl)-2-methoxy-phenyl]-acrylic acid 4-nitro-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: NaOH (1 equiv)

2: phosphorus trichloride

3: pyridine

With pyridine; sodium hydroxide; phosphorus trichloride;
DOI:10.1021/ja00522a054