2-(4'-nitrophenylazo)-5a-phenyl-6,6-dimethyl-5a,6-dihydro-12H-indolo[2,1-b][1,3]benzooxazine

Base Information

Chemical Name:2-(4'-nitrophenylazo)-5a-phenyl-6,6-dimethyl-5a,6-dihydro-12H-indolo[2,1-b][1,3]benzooxazine
CAS No.:872056-29-6
Molecular Formula:C₂₉H₂₄N₄O₃
Molecular Weight:476.535
Hs Code.:

Synonyms:2-(4'-nitrophenylazo)-5a-phenyl-6,6-dimethyl-5a,6-dihydro-12H-indolo[2,1-b][1,3]benzooxazine

Suppliers and Price of 2-(4'-nitrophenylazo)-5a-phenyl-6,6-dimethyl-5a,6-dihydro-12H-indolo[2,1-b][1,3]benzooxazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(4'-nitrophenylazo)-5a-phenyl-6,6-dimethyl-5a,6-dihydro-12H-indolo[2,1-b][1,3]benzooxazine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(4'-nitrophenylazo)-5a-phenyl-6,6-dimethyl-5a,6-dihydro-12H-indolo[2,1-b][1,3]benzooxazine

There total 5 articles about 2-(4'-nitrophenylazo)-5a-phenyl-6,6-dimethyl-5a,6-dihydro-12H-indolo[2,1-b][1,3]benzooxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 6636-32-4
3,3-dimethyl-2-phenyl-3H-indole

: 155850-91-2
2-hydroxymethyl-4-(4'-nitrophenylazo)phenol

: 872056-29-6
2-(4'-nitrophenylazo)-5a-phenyl-6,6-dimethyl-5a,6-dihydro-12H-indolo[2,1-b][1,3]benzooxazine

Guidance literature:: 2-hydroxymethyl-4-(4'-nitrophenylazo)phenol; With phosphorus tribromide; triethylamine; In acetonitrile; at 0 ℃; Reflux; Inert atmosphere;

3,3-dimethyl-2-phenyl-3H-indole; In acetonitrile; at 20 ℃; for 36h;

Reference yield:

: Br^(1-)*C₂₉H₂₅N₄O₃⁽¹⁺⁾

: 872056-29-6
2-(4'-nitrophenylazo)-5a-phenyl-6,6-dimethyl-5a,6-dihydro-12H-indolo[2,1-b][1,3]benzooxazine

Guidance literature:: With potassium hydroxide; In water;
DOI:10.1021/la201062h

Reference yield:

: 6636-32-4
3,3-dimethyl-2-phenyl-3H-indole

: 872056-29-6
2-(4'-nitrophenylazo)-5a-phenyl-6,6-dimethyl-5a,6-dihydro-12H-indolo[2,1-b][1,3]benzooxazine

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile

2: potassium hydroxide / water

With potassium hydroxide; In water; acetonitrile;
DOI:10.1021/la201062h