5-chloro-1,3-diformyl-2-hydroxybenzene bis(benzoylhydrazone)

Base Information

Chemical Name:5-chloro-1,3-diformyl-2-hydroxybenzene bis(benzoylhydrazone)
CAS No.:171566-59-9
Molecular Formula:C₂₂H₁₇ClN₄O₃
Molecular Weight:420.855
Hs Code.:

Synonyms:5-chloro-1,3-diformyl-2-hydroxybenzene bis(benzoylhydrazone)

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Chemical Property of 5-chloro-1,3-diformyl-2-hydroxybenzene bis(benzoylhydrazone)

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Technology Process of 5-chloro-1,3-diformyl-2-hydroxybenzene bis(benzoylhydrazone)

There total 1 articles about 5-chloro-1,3-diformyl-2-hydroxybenzene bis(benzoylhydrazone) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 32596-43-3
2,6-diformyl-4-chlorophenol

: 613-94-5
benzoic acid hydrazide

: 171566-59-9
5-chloro-1,3-diformyl-2-hydroxybenzene bis(benzoylhydrazone)

Guidance literature:: With acetic acid; In ethanol;
DOI:10.1016/j.poly.2012.06.025

Reference yield: 71.0%

: samarium nitrate hexahydrate water

: 171566-59-9
5-chloro-1,3-diformyl-2-hydroxybenzene bis(benzoylhydrazone)

: lithium chloride

: Sm₂((C₆H₅CONHNCH)2ClC₆H₂O)3⁽³⁺⁾*Cl^(1-)*2NO₃^(1-)*H₂O=[Sm₂((C₆H₅CONHNCH)2ClC₆H₂O)3]Cl(NO₃)2*H₂O

Guidance literature:: In methanol; soln. of Sm(NO3)3*7H2O in CH3OH added to suspn. of ligand in CH3OH (Ln:L=1:1.5), mixt. refluxed for 1 h, 3 equiv. of LiCl added; soln. filtered, filtrate kept at 298 K for 3 d, crystals filtered off; elem. anal.;
DOI:10.1016/j.poly.2012.06.025

Reference yield: 65.0%

: Nd⁽³⁺⁾*3NO₃^(1-)*7H₂O=Nd(NO₃)3*7H₂O

: 171566-59-9
5-chloro-1,3-diformyl-2-hydroxybenzene bis(benzoylhydrazone)

: lithium chloride

: Nd₂((C₆H₅CONHNCH)2ClC₆H₂O)3⁽³⁺⁾*Cl^(1-)*2NO₃^(1-)*2H₂O=[Nd₂((C₆H₅CONHNCH)2ClC₆H₂O)3]Cl(NO₃)2*2H₂O

Guidance literature:: In methanol; soln. of Nd(NO3)3*7H2O in CH3OH added to suspn. of ligand in CH3OH (Ln:L=1:1.5), mixt. refluxed for 1 h, 3 equiv. of LiCl added; soln. filtered, filtrate kept at 298 K for 3 d, crystals filtered off; elem. anal.;
DOI:10.1016/j.poly.2012.06.025