2-methoxy-1-(3-methyl-but-2-enyl)-cyclohexa-2,5-diene-1-carboxylic acid methyl ester

Base Information

Chemical Name:2-methoxy-1-(3-methyl-but-2-enyl)-cyclohexa-2,5-diene-1-carboxylic acid methyl ester
CAS No.:1015779-41-5
Molecular Formula:C₁₄H₂₀O₃
Molecular Weight:236.311
Hs Code.:

Synonyms:2-methoxy-1-(3-methyl-but-2-enyl)-cyclohexa-2,5-diene-1-carboxylic acid methyl ester

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Chemical Property of 2-methoxy-1-(3-methyl-but-2-enyl)-cyclohexa-2,5-diene-1-carboxylic acid methyl ester

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Technology Process of 2-methoxy-1-(3-methyl-but-2-enyl)-cyclohexa-2,5-diene-1-carboxylic acid methyl ester

There total 2 articles about 2-methoxy-1-(3-methyl-but-2-enyl)-cyclohexa-2,5-diene-1-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 606-45-1
2-methoxybenzoic acid methyl ester

: 870-63-3
prenyl bromide

: 1015779-41-5
2-methoxy-1-(3-methyl-but-2-enyl)-cyclohexa-2,5-diene-1-carboxylic acid methyl ester

Guidance literature:: 2-methoxybenzoic acid methyl ester; With ammonia; potassium; In tert-butyl alcohol; at -78 ℃; for 0.0833333h; Inert atmosphere;

prenyl bromide; With penta-1,3-diene; lithium iodide; In tetrahydrofuran; tert-butyl alcohol; at -78 - 25 ℃;
DOI:10.1021/ol800118c

Reference yield: 77.0%

: 606-45-1
2-methoxybenzoic acid methyl ester

: 870-63-3
prenyl bromide

: 1015779-41-5
2-methoxy-1-(3-methyl-but-2-enyl)-cyclohexa-2,5-diene-1-carboxylic acid methyl ester

: methyl 3-(3-methyl-2-butenyl)-6-methoxy-1,5-cyclohexadiene-carboxylate

Guidance literature:: 2-methoxybenzoic acid methyl ester; With penta-1,3-diene; ammonia; potassium; In tert-butyl alcohol; at -78 ℃;

With lithium iodide; In tert-butyl alcohol; at -78 ℃; for 1h;

prenyl bromide; In tert-butyl alcohol; at -78 - 25 ℃;
DOI:10.1021/jo8015743