benzyl 2-acetamido-2-deoxy-6-O-mesyl-3-O--α-D-glucopyranoside

Base Information

• Chemical Name: benzyl 2-acetamido-2-deoxy-6-O-mesyl-3-O--α-D-glucopyranoside
• CAS No.: 74221-00-4
• Molecular Formula: C₂₀H₂₉NO₁₀S
• Molecular Weight: 475.517

Synonyms:benzyl 2-acetamido-2-deoxy-6-O-mesyl-3-O--α-D-glucopyranoside

Chemical Property of benzyl 2-acetamido-2-deoxy-6-O-mesyl-3-O--α-D-glucopyranoside

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Technology Process of benzyl 2-acetamido-2-deoxy-6-O-mesyl-3-O--α-D-glucopyranoside

There total 4 articles about benzyl 2-acetamido-2-deoxy-6-O-mesyl-3-O--α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

methanesulfonyl chloride (124-63-0) + benzyl 2-acetamido-2-deoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-α-D-glucopyranoside (40269-09-8) → benzyl 2-acetamido-2-deoxy-6-O-mesyl-3-O--α-D-glucopyranoside (74221-00-4)

Guidance literature:

With pyridine; at -20 ℃; for 5h;

DOI:10.1080/00021369.1980.10864112

Reference yield: 85.0%

benzyl 2-acetamido-2-deoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-α-D-glucopyranoside (40269-09-8) → benzyl 2-acetamido-2-deoxy-6-O-mesyl-3-O--α-D-glucopyranoside (74221-00-4)

Guidance literature:

DOI:10.1016/S0008-6215(00)85146-0

Reference yield:

benzyl 2-acetamido-2-deoxy-3-O--α-D-glucopyranoside (909889-92-5) + methanesulfonyl chloride (124-63-0) → benzyl 2-acetamido-2-deoxy-6-O-mesyl-3-O--α-D-glucopyranoside (74221-00-4)

Guidance literature:

In pyridine; water;

upstream raw materials:

methanesulfonyl chloride

benzyl 2-acetamido-2-deoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-α-D-glucopyranoside

(R)-2-(((4aR,6S,7R,8R,8aS)-7-acetamido-6-(benzyloxy)-2,2-dimethylhexahydropyrano[3,2-d][1,3]dioxin-8-yl)oxy)propanoic acid

benzyl 2-acetamido-2-deoxy-3-O--α-D-glucopyranoside

Downstream raw materials:

N-<2-O-(benzyl 2-acetamido-6-chloro-2,3,6-trideoxy-α-D-glucopyranoside-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamine benzyl ester

2-((2S,3R,4R,5S,6S)-3-Acetylamino-2-benzyloxy-6-chloromethyl-5-hydroxy-tetrahydro-pyran-4-yloxy)-propionic acid

benzyl 2-acetamido-6-chloro-2,6-dideoxy-3-O--α-D-glucopyranoside

(R)-2-((2S,3R,4R,5S,6R)-3-Acetylamino-5-azido-6-azidomethyl-2-benzyloxy-tetrahydro-pyran-4-yloxy)-propionic acid

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