1-(4-methoxyphenyl)-2-{4-[2-(piperidin-1-yl)ethoxy]phenyl}-1-(6-methoxynaphthalen-2-yl)propene

Base Information

Chemical Name:1-(4-methoxyphenyl)-2-{4-[2-(piperidin-1-yl)ethoxy]phenyl}-1-(6-methoxynaphthalen-2-yl)propene
CAS No.:848073-47-2
Molecular Formula:C₃₄H₃₇NO₃
Molecular Weight:507.673
Hs Code.:

Synonyms:1-(4-methoxyphenyl)-2-{4-[2-(piperidin-1-yl)ethoxy]phenyl}-1-(6-methoxynaphthalen-2-yl)propene

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Chemical Property of 1-(4-methoxyphenyl)-2-{4-[2-(piperidin-1-yl)ethoxy]phenyl}-1-(6-methoxynaphthalen-2-yl)propene

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Technology Process of 1-(4-methoxyphenyl)-2-{4-[2-(piperidin-1-yl)ethoxy]phenyl}-1-(6-methoxynaphthalen-2-yl)propene

There total 4 articles about 1-(4-methoxyphenyl)-2-{4-[2-(piperidin-1-yl)ethoxy]phenyl}-1-(6-methoxynaphthalen-2-yl)propene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₄H₃₉NO₄

: 848073-47-2
1-(4-methoxyphenyl)-2-{4-[2-(piperidin-1-yl)ethoxy]phenyl}-1-(6-methoxynaphthalen-2-yl)propene

Guidance literature:: With hydrogenchloride; In methanol; for 1h; Heating;
DOI:10.1016/j.bmc.2004.11.051

Reference yield:

: 848073-45-0
1-(4-methoxyphenyl)-2-[4-(2-(piperidin-1-yl)ethoxy)phenyl]propan-1-one

: 848073-47-2
1-(4-methoxyphenyl)-2-{4-[2-(piperidin-1-yl)ethoxy]phenyl}-1-(6-methoxynaphthalen-2-yl)propene

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / tetrahydrofuran; cyclohexane / 0.08 h / -78 °C

1.2: tetrahydrofuran; cyclohexane / 1 h / -78 - 20 °C

2.1: 0.21 g / aq. HCl / methanol / 1 h / Heating

With hydrogenchloride; n-butyllithium; In tetrahydrofuran; methanol; cyclohexane;
DOI:10.1016/j.bmc.2004.11.051

Reference yield:

: 35258-41-4
1,2-bis-(4-methoxy-phenyl)-propan-1-one

: 848073-47-2
1-(4-methoxyphenyl)-2-{4-[2-(piperidin-1-yl)ethoxy]phenyl}-1-(6-methoxynaphthalen-2-yl)propene

Guidance literature:: Multi-step reaction with 4 steps

1.1: 88 percent / BBr₃ / CH₂Cl₂

2.1: 45 percent / Na / ethanol / 1 h / Heating

3.1: n-BuLi / tetrahydrofuran; cyclohexane / 0.08 h / -78 °C

3.2: tetrahydrofuran; cyclohexane / 1 h / -78 - 20 °C

4.1: 0.21 g / aq. HCl / methanol / 1 h / Heating

With hydrogenchloride; n-butyllithium; sodium; boron tribromide; In tetrahydrofuran; methanol; ethanol; dichloromethane; cyclohexane;
DOI:10.1016/j.bmc.2004.11.051