(Z)-2-Acetylamino-N-((S)-1-benzyloxymethyl-3-methylsulfanyl-propyl)-3-phenyl-acrylamide

Base Information

Chemical Name:(Z)-2-Acetylamino-N-((S)-1-benzyloxymethyl-3-methylsulfanyl-propyl)-3-phenyl-acrylamide
CAS No.:84274-36-2
Molecular Formula:C₂₃H₂₈N₂O₃S
Molecular Weight:412.553
Hs Code.:

Synonyms:(Z)-2-Acetylamino-N-((S)-1-benzyloxymethyl-3-methylsulfanyl-propyl)-3-phenyl-acrylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-Acetylamino-N-((S)-1-benzyloxymethyl-3-methylsulfanyl-propyl)-3-phenyl-acrylamide

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Technology Process of (Z)-2-Acetylamino-N-((S)-1-benzyloxymethyl-3-methylsulfanyl-propyl)-3-phenyl-acrylamide

There total 1 articles about (Z)-2-Acetylamino-N-((S)-1-benzyloxymethyl-3-methylsulfanyl-propyl)-3-phenyl-acrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 93200-01-2
(S)-menthioninol benzyl ether

: 38879-46-8
(Z)-4-benzylidene-2-methyl-5(4H)-oxazolone

: 84274-36-2
(Z)-2-Acetylamino-N-((S)-1-benzyloxymethyl-3-methylsulfanyl-propyl)-3-phenyl-acrylamide

Guidance literature:: With triethylamine; In chloroform; Ambient temperature;
DOI:10.1016/S0040-4020(01)82412-1

Reference yield: 4.5%

: 84274-36-2
(Z)-2-Acetylamino-N-((S)-1-benzyloxymethyl-3-methylsulfanyl-propyl)-3-phenyl-acrylamide

: 84274-43-1
(R)-2-Acetylamino-N-((S)-1-benzyloxymethyl-3-methylsulfanyl-propyl)-3-phenyl-propionamide

: 84274-44-2
(S)-2-Acetylamino-N-((S)-1-benzyloxymethyl-3-methylsulfanyl-propyl)-3-phenyl-propionamide

Guidance literature:: With hydrogen; <(+)BPPM>ClO4; In ethanol; at 40 ℃; for 46h; under 3800 Torr; Yield given;
DOI:10.1246/cl.1982.1335

Reference yield:

: 84274-36-2
(Z)-2-Acetylamino-N-((S)-1-benzyloxymethyl-3-methylsulfanyl-propyl)-3-phenyl-acrylamide

: 84274-50-0,84274-51-1
2-Acetylamino-N-((S)-1-hydroxymethyl-3-methylsulfanyl-propyl)-3-phenyl-propionamide

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / <((+)BPPM)Rh(norbornadiene)>⁽¹⁺⁾*ClO₄^(1-) / ethanol / 46 h / 40 °C / 3800 Torr

2: 1.) HBr; 2.) 1N NaOH / 1.) AcOH

With sodium hydroxide; hydrogen bromide; hydrogen; <((-)BPPM)Rh(norbornadiene)>(1+)*ClO4(1-); In ethanol;
DOI:10.1016/S0040-4020(01)82412-1