N,N-di(chloromethyl)-4-formylaniline

Base Information

Chemical Name:N,N-di(chloromethyl)-4-formylaniline
CAS No.:882574-04-1
Molecular Formula:C₉H₉Cl₂NO
Molecular Weight:218.083
Hs Code.:

Synonyms:N,N-di(chloromethyl)-4-formylaniline

Suppliers and Price of N,N-di(chloromethyl)-4-formylaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 15 raw suppliers

Chemical Property of N,N-di(chloromethyl)-4-formylaniline

Chemical Property:

Purity/Quality:: 99% ,98%,Electron Grade , ^*data from raw suppliers

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Technology Process of N,N-di(chloromethyl)-4-formylaniline

There total 1 articles about N,N-di(chloromethyl)-4-formylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 556-18-3,28107-09-7
4-aminobenzaldehyde

: 882574-04-1
N,N-di(chloromethyl)-4-formylaniline

Guidance literature:: formaldehyd; 4-aminobenzaldehyde; In dichloromethane; at 20 ℃; for 5h;

With thionyl chloride; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1002/anie.200503602

Reference yield: 41.0%

: 882574-04-1
N,N-di(chloromethyl)-4-formylaniline

: bis(μ-mercapto)bis(tricarbonyliron)

: [(μ-SCH2)2N(C6H4CHO-p)]Fe2(CO)6

Guidance literature:: With triethylamine; In tetrahydrofuran; at -78 - 20 ℃; for 12.5h;

Reference yield: 32.0%

: 882574-04-1
N,N-di(chloromethyl)-4-formylaniline

: Fe2(μ-S)2(CO)6

: 76-05-1
trifluoroacetic acid

: [(μ-SCH2)2N(C6H4CHO-p)]Fe2(CO)6

Guidance literature:: With lithium triethylborohydride; In tetrahydrofuran; a soln. of Li-contg. compd. (17.0 mmol) in THF was added to a soln. of Fe2-contg. compd. (8.5 mmol) in THF at -78°C; CF3CO2H (17.0 mmol) and CHOC6H4N(CH2Cl)2 (8.5 mmol) were then added; stirring at this temp. for 0.5 h and at room temp. for 12 h; the volatiles were removed under vac.; TLC (CH2Cl2/petroleum ether (2:1,v/v) as eluent); elem. anal.;
DOI:10.1002/anie.200503602