N-<2-(3,4-dimethoxyphenyl)ethyl>-N-(3-oxo-1-cyclohexen-1-yl)-α-(methylthio)acetamide

Base Information

Chemical Name:N-<2-(3,4-dimethoxyphenyl)ethyl>-N-(3-oxo-1-cyclohexen-1-yl)-α-(methylthio)acetamide
CAS No.:107199-45-1
Molecular Formula:C₁₉H₂₅NO₄S
Molecular Weight:363.478
Hs Code.:

Synonyms:N-<2-(3,4-dimethoxyphenyl)ethyl>-N-(3-oxo-1-cyclohexen-1-yl)-α-(methylthio)acetamide

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Chemical Property of N-<2-(3,4-dimethoxyphenyl)ethyl>-N-(3-oxo-1-cyclohexen-1-yl)-α-(methylthio)acetamide

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Technology Process of N-<2-(3,4-dimethoxyphenyl)ethyl>-N-(3-oxo-1-cyclohexen-1-yl)-α-(methylthio)acetamide

There total 1 articles about N-<2-(3,4-dimethoxyphenyl)ethyl>-N-(3-oxo-1-cyclohexen-1-yl)-α-(methylthio)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 63521-90-4
α-(methylthio)acetic acid anhydride

: 27032-09-3
3-<2-(3,4-Dimethoxyphenyl)ethylamino>-2-cyclohexen-1-on

: 107199-45-1
N-<2-(3,4-dimethoxyphenyl)ethyl>-N-(3-oxo-1-cyclohexen-1-yl)-α-(methylthio)acetamide

Guidance literature:: With pyridine; at 70 - 80 ℃; for 1h;

Reference yield: 87.0%

: 107199-45-1
N-<2-(3,4-dimethoxyphenyl)ethyl>-N-(3-oxo-1-cyclohexen-1-yl)-α-(methylthio)acetamide

: 107199-47-3
N-<2-(3,4-dimethoxyphenyl)ethyl>-N-(3-oxo-1-cyclohexen-1-yl)-α-(methylsulfinyl)acetamide

Guidance literature:: With sodium periodate; In methanol; water; for 10h; Ambient temperature;

Reference yield:

: 107199-45-1
N-<2-(3,4-dimethoxyphenyl)ethyl>-N-(3-oxo-1-cyclohexen-1-yl)-α-(methylthio)acetamide

: 107199-50-8
3,5,6,7-tetrahydro-1-<2-(3,4-dimethoxyphenyl)ethyl>-3-methylthio-1H-indole-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / sodium metaperiodate / H₂O; methanol / 10 h / Ambient temperature

2: 75 percent / p-toluenesulfonic acid / 1,2-dichloro-ethane / 0.25 h / Heating

With sodium periodate; toluene-4-sulfonic acid; In methanol; water; 1,2-dichloro-ethane;