(11Z,13E)-15-hydroxyicosa-11,13-dienoic acid

Base Information

Chemical Name:(11Z,13E)-15-hydroxyicosa-11,13-dienoic acid
CAS No.:77159-57-0
Molecular Formula:C₂₀H₃₆O₃
Molecular Weight:324.504
Hs Code.:2918199090
ChEMBL ID:CHEMBL420428
DSSTox Substance ID:DTXSID20274307
Metabolomics Workbench ID:66149
Wikidata:Q27140187
Mol file:77159-57-0.mol

Synonyms:77159-57-0;(11Z,13E)-15-hydroxyicosa-11,13-dienoic acid;15-hydroxy-11Z,13E-eicosadienoic acid;15-HEDE;CHEMBL420428;CHEBI:72847;(+-)-15-HEDE;(+/-)-15-Hydroxy-11Z,13E-eicosadienoic acid;11,13-Eicosadienoicacid, 15-hydroxy-, (11Z,13E)-;DTXSID20274307;ZTRWPEHMGCHTIT-QWAPPMFBSA-N;(??)15-HEDE;BDBM50025739;AKOS027383855;15-hydroxy-11(Z),13(E)-eicosadienoic acid;15-Hydroxy-icosa-11,13-dienoic acid(15-HEDE);SR-01000946942;(11Z,13E)-15-Hydroxy-11,13-icosadienoic acid;SR-01000946942-1;Q27140187;(S)-15-Hydroxy-icosa-11,13-dienoic acid(15(S)-OH-20 : 2)

Suppliers and Price of (11Z,13E)-15-hydroxyicosa-11,13-dienoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Cayman Chemical
(±)15-HEDE ≥98%
250μg
$ 322.00

Cayman Chemical
(±)15-HEDE ≥98%
100μg
$ 137.00

Cayman Chemical
(±)15-HEDE ≥98%
50μg
$ 74.00

Cayman Chemical
(±)15-HEDE ≥98%
25μg
$ 39.00

AHH
(+/-)-15-Hydroxy-11Z,13E-eicosadienoic acid 98%
0.001g
$ 920.00

Total 4 raw suppliers

Chemical Property of (11Z,13E)-15-hydroxyicosa-11,13-dienoic acid

Chemical Property:

PSA：57.53000
LogP:5.63550
XLogP3:6.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:16
Exact Mass:324.26644501
Heavy Atom Count:23
Complexity:321

Purity/Quality:

99% ^*data from raw suppliers

(±)15-HEDE ≥98% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCC(C=CC=CCCCCCCCCCC(=O)O)O
Isomeric SMILES:CCCCCC(/C=C/C=C\CCCCCCCCCC(=O)O)O

Technology Process of (11Z,13E)-15-hydroxyicosa-11,13-dienoic acid

There total 4 articles about (11Z,13E)-15-hydroxyicosa-11,13-dienoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 105835-54-9
(13E)-15-hydroxyeicosa-13-en-11-ynoic acid

: 77159-57-0,92693-04-4
15-hydroxy-11Z,13E-eicosadienoic acid

: (11Z)-15-hydroxyeicosa-11-enoic acid

Guidance literature:: With quinoline; hydrogen; Pd-BaSO₄; In ethyl acetate; under 760 Torr; Ambient temperature;
DOI:10.1021/jm00385a005

Reference yield:

: 16900-60-0
dodec-11-ynoic acid

: 77159-57-0,92693-04-4
15-hydroxy-11Z,13E-eicosadienoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / CuI, tetrakis(triphenylphosphine)palladium / diethylamine / 3 h / Ambient temperature

2: 30 percent / H₂, quinoline / 10percent Pd/BaSO₄ / ethyl acetate / 760 Torr / Ambient temperature

With quinoline; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydrogen; Pd-BaSO₄; In ethyl acetate; diethylamine;
DOI:10.1021/jm00385a005

Reference yield:

: 39178-65-9
(E)-1-iodooct-1-en-3-ol

: 77159-57-0,92693-04-4
15-hydroxy-11Z,13E-eicosadienoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / CuI, tetrakis(triphenylphosphine)palladium / diethylamine / 3 h / Ambient temperature

2: 30 percent / H₂, quinoline / 10percent Pd/BaSO₄ / ethyl acetate / 760 Torr / Ambient temperature

With quinoline; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydrogen; Pd-BaSO₄; In ethyl acetate; diethylamine;
DOI:10.1021/jm00385a005